Christian MASQUELIER @ LRCS - Amiens
Christian MASQUELIER          @ LRCS - Amiens

Publications in peer-reviewed Journals

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177.  Zirconia-free NaSICON Solid Electrolyte Materials for Sodium All-solid-state Batteries

A. Tieu, E. Mahayoni, Y. Li, Z. Deng, F. Fauth, J.N. Chotard, V. Seznec, S. Adams, C. Masquelier, P. Canepa

J. Materials Chemistry A, 11, 23233-23242 (2023) ; DOI : 10.1039/D3TA04665F


176. Dynamic Lone Pairs and Fluoride-Ion Disorder in Cubic-BaSnF4

B. Mercadier, S. W. Coles, M. Duttine, C. Legein, M. Body, O. Borkiewicz, O. Lebedev, B.J. Morgan, C. Masquelier, D. Dambournet

J. Amer. Chem. Soc., 145, 43, 23739-23754 (2023) ; DOI : 10.1021/jacs.3c08232


175. Thermal stability of Na3-xV2(PO4)2F3-yOy: influence of F- for O2- substitution and degradation mechanisms

C. Pablos J. Olchowka, E. Petit, G. Minart, M. Duttine, F. Weill, C. Masquelier, D. Carlier, L.Croguennec

Chem. Mater.,  25(10), 4078-4088 (2023) ; DOI : 10.1021/acs.chemmater.3c00539


174. Irreversible Electrochemical Reaction at High Voltage Induced by Distortion of Mn and V Structural Environments in Na4MnV(PO4)3

S. Park, J.N. Chotard, D. Carlier, F. Fauth, A. Iadecola, C. Masquelier, L. Croguennec

Chem. Mater., 35(8), 3181-3195 (2023) ; DOI : 10.1021/acs.chemmater.2c03787


173. Theoretical and Experimental Studies of ion Transport in Mixed Polyanion Solid Electrolytes

Z. Deng, T. P. Mishra, E. Mahayoni, J.N. Chotard, V. Seznec, A. K. Cheetham, C. Masquelier, G. S. Gautam & P. Canepa

Nature Communications, 13, 4470 (2022) ; DOI : 10.1038/s41467-022-32190-7


172. Feasibility and Limitations of High-Voltage Lithium-Iron-Manganese Spinels

A. Windmüller, T. Renzi, H. Kungl, S. Taranenko, E. Suard, F. Fauth, M. Duttine, C. Tsai, R. Sun, Y. Durmus, H. Tempel, P. Jakes, C. Masquelier, R. Eichel, L. Croguennec & H. Ehrenberg

J. Electrochem. Soc., 169(7), 070518 (2022) ; DOI : 10.1149/1945-7111/ac7ef8


171.  An asymmetric Sodium Extraction/Insertion Mechanism for the Fe/V-mixed NASICON Na4FeV(PO4)3

S. Park, J. N. Chotard, D. Carlier, I. Moog, M. Duttine, F. Fauth, A. Iadecola, L. Croguennec & C. Masquelier

Published as part of the Virtual Special Issue “John Goodenough at 100”.

Chem. Mater., 34(9), 4142-4152 (2022) ; DOI : 10.1021/acs.chemmater.2c00501


170. Two-dimensional substitution series Na3P1−xSbxPS4-ySey – beyond static description of structural bottlenecks for Na+ transport

P. Till, M. Agne, M. Kraft, M. Courty, T. Famprikis, M. Ghidiu, T. Krauskopf, C. Masquelier, W. Zeier,

Chem. Mater. 34(5), 2410-2421 (2022) ; DOI : 10.1021/acs.chemmater.1c04445


169. Phase Stability and Sodium-Vacancy Orderings in a NaSICON Electrode

Z. Wang, S. Park, Z. Deng, F. Fauth, D. Carlier, L. Croguennec, C. Masquelier, J. N. Chotard, P. Canepa,

J. Mater. Chem. A., 10, 209-217 (2022) ; DOI : 10.1039/D1TA09249A


168.  Structural details in Li3PS4: variety in thiophosphate building blocks and correlation to ion transport

Ö. U. Kudu, T. Famprikis, S. Cretu, B. Porcheron, E. Salager, A. Demortiere, M. Courty, V. Viallet, T. Le Mercier, B. Fleutot, M.D. Braida & C. Masquelier

Energy Storage Materials, 44, 168-179 (2022) ; DOI : 10.1016/j.ensm.2021.10.021


167.  Crystal Structure of the Intermediate Na2V2(PO4)3 Phase and Electrochemical Reaction Mechanisms in the NaxV2(PO4)3 (1 ≤ x ≤ 4) System

S. Park, Z. Wang, Z. Deng, I. Moog, P. Canepa, F. Fauth, D. Carlier, L. Croguennec, C. Masquelier,  J. N. Chotard

Chem. Mater. , 34, 451-462 (2021) ; DOI : 10.1021/acs.chemmater.1c04033 


166. Crystal Structures and Local Environments of NASICON-type Na3FeV(PO4)3 and Na4FeV(PO4)3 Positive Electrode Materials for Na-ion Batteries

S. Park, J. N. Chotard, D. Carlier, I. Moog, M. Courty, M. Duttine, F. Fauth, A. Iadecola, L. Croguennec & C. Masquelier

Chem. Mater. (2021) ; DOI : 10.1021/acs.chemmater.1c01457


165. Polyanionic-type compoubds as positive electrodes for Na-Ion Batteries

L.H.B. Nguyen, F. Chen, C. Masquelier & L. Croguennec

Na-Ion Batteries, First Edition, L. Monconduit & L. Croguennec, pp. 47-100, John Wiley & Sons (2021)


164. Insights into the rich polymorphism of the Na+ ion conductor Na3PS4 from the perspective of variable-temperature diffraction and spectroscopy

T. Famprikis, H. Bouyanfif, P. Canepa, M. Zbiri, J. Dawson, E. Suard, F. Fauth, H. Playford, D. Dambournet, O. Borkiewicz, M. Courty, O. Clemens, J.N. Chotard, M.S. Islam & C. Masquelier

Chem. Mater. , 33(14), 5652-5667 (2021) ; DOI : 10.1021/acs.chemmater.1c01113


163. Towards high-voltage multi-electron reactions in Alkali-ion batteries using vanadium phosphate cathodes: a review

E. Boivin, C. Masquelier, L. Croguennec

Molecules, 26(5), 1428 (2021) ; DOI : 10.3390/molecules26051428


162. A Chemical Map of NaSiCON Electrode Materials for Sodium-ion Batteries

B. Singh, Z. Wang, S. Park, G. Sai Gautam, J.N. Chotard, L. Croguennec, D. Carlier, A. K. Cheetham, C. Masquelier & P. Canepa

J. Mater. Chem. A, 9(1), 281-292 (2021) ; DOI : 10.1039/d0ta10688


161. Challenges of today for Na-based batteries of the future

P. Adelhelm, M. Casas-Cabanas, L. Croguennec, I. Hasa, A. Koposov, S. Mariyappan, C. Masquelier & D. Saurel

J. Power Sources482, 228872 (2021) ; DOI : 10.1016/j.jpowsour.2020.228872


160. Ionothermal Synthesis of Polyanionic Electrode Material Na3V2(PO4)2FO2 Through Topotactic Reaction

J. Olchowka, L. H.B. Nguyen, E. Petit, P. Sanz Camacho, M. Duttine, C. Masquelier, D. Carlier, L. Croguennec

Inorg. Chem., 53(23), 17282-17290 (2020) ; DOI : 10.1021/acs.inorgchem.0c02546


159. A Combined Operando Synchrotron X‑ray Absorption Spectroscopy and First-Principles Density Functional Theory Study to Unravel the Vanadium Redox Paradox in the Na3V2(PO4)2F3 − Na3V2(PO4)2FO2 Compositions.

L. Nguyen, A. Iadecola, S. Belin, J. Olchowka, C. Masquelier, D. Carlier & L. Croguennec

J. Phys. Chem. C., 124(43), 23511-23522 (2020) ; DOI : 10.1021/acs.jpcc.0c06967


158. Enumeration as tool for structure solution – a materials genomic approach to solving the 100 K structure of Na3V2(PO4)2F3

G. S. Mattei, J. M. Dagdelen, M. Bianchini, N. Zimmerman, E. Suard, F. Fauth, C. Masquelier, L. Croguennec, G. Ceder, K. A. Persson & P. G. Khalifah

Chem. Mater., 32(18), 7908-7920 (2020) ; DOI : 10.1021/acs.chemmater.0c03190


157. Na7V3(P2O7)4 as a high voltage electrode material for Na-ion batteries: crystal structure and mechanism of Na+ extraction/insertion by operando X-ray diffraction

V. M. Kovrugin, J.N. Chotard, F. Fauth & C. Masquelier

J. Mater. Chem. A., 8, 21110-21121 (2020) ; DOI : 10.1039/d0ta06230h


156. Under Pressure: Mechanical Effects on Ion Conduction in Na3PS4

T. Famprikis, U. Kudu, J. Dawson, P. Canepa, F. Fauth, E. Suard, M. Zbiri, D. Dambournet, O. Borkiewicz, H. Bouyanfif, S. Emge, C. Grey, S. Cretu, J.N. Chotard, W. Zeier, M. S. Islam & C. Masquelier

J. Amer. Chem. Soc., 142(43), 18422-18436 (2020) ; DOI : 10.1021/jacs.0c06668


155. Phase Behavior in NaSiCON Electrolytes and Electrodes

Z. Deng, G. Sai Gautam, S. Krishna Kolli, J. N. Chotard, A. K. Cheetham, C. Masquelier & P. Canepa

Chem. Mater. 32, 7908-7920 (2020)DOI: 10.1021/acs.chemmater.0c02695


154. Mechanochemical Synthesis and Ion Transport properties of Na3OX (X = Cl, Br, I and/or BH4) Antiperovskite Solid Electrolytes

E. Ahiavi, J.A. Dawson, U. Kudu, M. Courty, S. Islam, O. Clemens, C. Masquelier, T. Famprikis

J. Power Sources, 471, 228489 (2020) ; DOI : 10.1016/j.jpowsour.2020.228489


153. Local atomic and electronic structure in the LiVPO4(F,O) Tavorite‐type materials from Solid State NMR combined with DFT calculations

T. Bamine, E. Boivin, C. Masquelier, L. Croguennec, E. Salager, D. Carlier

Mag. Res. Chemistry, 58, 1109-1117 (2020) ; DOI : 10.1002/mrc.5059


152. HBO2 as an adhesive agent for the multi-step fabrication of  All-Solid-State Sodium Batteries

T. Kobayashi, F. Chen, V. Seznec, C. Masquelier

J. Power Sources, 450, 227597 (2020) ; DOI: 10.1016/j.jpowsour.2019.227597


151. Density Functional Theory-Assisted P-31 and Na-23 Magic-Angle Spinning Nuclear Magnetic Resonance Study of the Na3V2(PO4)2F3-Na3V2(PO4)2FO2 Solid Solution: Unraveling Its Local and Electronic Structures

L. H. B. Nguyen, P. Sanz Camacho, T. Broux, J. Olchowka, C. Masquelier, L. Croguennec & D. Carlier

Chem. Mater., 31, 9759-9768 (2019) ; DOI : 10.1021/acs.chemmater.9b03546 


150. A new plastic polymorph of the Na+ ion conductor Na3PS4

T. Famprikis, F. Fauth, E. Suard, B. Fleutot, M. Courty, J. N. Chotard, S. Islam & C. Masquelier

ACS Materials Letters, 1, 641-646 (2019) ; DOI: 10.1021/acsmaterialslett.9b00322


149. Monitoring the crystal structure and the electrochemical properties of Na3(VO)2(PO4)2F through Fe3+-substitution

L. H.B. Nguyen, J. Olchowka, S. Belin, P. S. Camacho, M. Duttine, A. Iadecola, F. Fauth, D. Carlier, C. Masquelier & L. Croguennec

ACS Applied Materials & Interfaces (2019) ; DOI: 10.1021/acsami.9b14249


148. Substitution of Aluminium for Vanadium in the Na-ion battery positive electrode material Na3V2(PO4)2F3

J. Olchowka, L. H. B. Nguyen, T. Broux, P.S. Camacho, E. Petit, F. Fauth, D. Carlier, C. Masquelier & L. Croguennec

Chem. Comm, 55, 11719 (2019) ; DOI: 10.1039/c9cc05137f


147. On the high-temperature behavior of the Na+ ion conductor Na3PS4

T. Famprikis, F. Fauth, E. Suard, B. Fleutot, M. Courty, J. N. Chotard, S. Islam & C. Masquelier

Open source paper in ChemRXIV (2019) ; DOI: 10.26434/chemrxiv.8003707


146. The redox paradox of Vanadium in Tavorite LiVPO4F1-yOy

E. Boivin, R. David, J. N. Chotard, T. Bamine, A. Iadecola, L Bourgeois, E. Suard, F. Fauth, D. Carlier, C. Masquelier & L. Croguennec

Chem. Mater., 31, 7367-7373 (2019) ; DOI: 10.1021/acs.chemmater.9b01987


145. Fundamentals of Inorganic Solid‑State Electrolytes for Batteries

T. Famprikis, P. Canepa, J. A. Dawson, M. S. Islam & C. Masquelier

Nature Materials (2019) ; DOI: 10.1038/s41563-019-0431-3


144. Stability in water and electrochemical properties of compositions in the Na3V2(PO4)2F3 – Na3(VO)2(PO4)2F solid solution

L. H. B. Nguyen, T. Broux , P. S. Camacho, D. Denux, L. Bourgeois, S. Belin, A. Iadecola, F. Fauth, D. Carlier, J. Olchowka, C. Masquelier & L. Croguennec

Energy Storage Materials, 20, 324-334 (2019) ; DOI: 10.1016/J.ensm.2019.04.010


143. High Rate Performance for Optimized Carbon Coated Na3V2(PO4)2F3 in Na-ion batteries

T. Broux, F. Fauth, N. Hall, M. Bianchini, T. Bamine, J.-B. Leriche, E. Suard, D. Carlier, L. Simonin, C. Masquelier & L. Croguennec

Small Methods, 3, 1800215 (2019) ; DOI: 10.1002/smtd.201800215


142.  A NASICON-type positive electrode for Na batteries with high energy density : Na4MnV(PO4)3

F. Chen, V. Kovrugin, R. David, J. N. Chotard, O. Mentré, F. Fauth & C. Masquelier

Small Methods, 3, 1800218 (2019) ; DOI: 10.1002/smtd.201800218


141. Mineral-inspired crystal growth of Na2Cu(SO4)2: structure, physical properties, and polymorphism of Na2M(SO4)2 compounds

V.M. Kovrugin, D.O. Nekrasova, O.I. Siidra, O. Mentré, C. Masquelier, M. Colmont, S. Stefanovich, S. Yu. & S. Colis

Crystal Growth and Design, 19(2), 1233-1244 (2019) ; DOI10.1021/acs.cgd.8b01658


140.  A Review of Structural Properties and Synthesis Methods of Solid Electrolyte Materials in the Li2S – P2S5 Binary System

Ö. U. Kudu, T. Famprikis, B. Fleutot, M. D. Braida, T. Le Mercier,  M. S. Islam & C. Masquelier

J. Power Sources, J. Power Sources, 407, 31-43 (2018) ; 


139. LiVPO4F1-yOy Tavorite-type compositions: Influence of the vanadyl-type defects’ concentration on the structure and electrochemical performances

E. Boivin, R. David, J. N. Chotard, T. Bamine, A. Iadecola, L Bourgeois, E. Suard, F. Fauth, D. Carlier, C. Masquelier & L. Croguennec

Chem. Mater., 30(16), 5682-5693 (2018) ; DOI: 10.1021/acs.chemmater.8b02138


138. Structural transformation induced by electrochemical Na+ extraction from a new high potential cathode material: Na3V(PO4)2

V. Kovrugin, R. David, J.N. Chotard, N. Recham & C. Masquelier

Inorg. Chem., 57(15), 8760-8768 (2018) ; DOI: 10.1021/acs.inorgchem.8b00401


137. Ag+ ion exchange into the polyanionic framework of Na3V2(PO4)2F3

M. Bianchini, F. Lalere, F. Fauth, L. Croguennec & C. Masquelier

J. Mater. Chem. A., 6, 10340-10347 (2018) ; DOI: 10.1039/C8TA01095A


136. Crystal structures, local atomic environments and ion diffusion mechanisms of scandium-substituted NASICON solid electrolytes

Y. Deng, C. Eames, L. H. B. Nguyen, O. Pecher, K. J. Griffith, M. Courty, B. Fleutot, J. N. Chotard, C. P. Grey, M. S. Islam & C. Masquelier

Chem. Mater., 30(8), 2618-2630 (2018) ; DOI: 10.1021/acs.chemmater.7b05237


135. Coupled X-ray diffraction and electrochemical studies of the mixed Ti/V-containing NASICON: Na2TiV(PO4)3

F. Lalère, V. Seznec, M. Courty, J. N. Chotard & C. Masquelier

J. Mater. Chem. A, 6, 6654-6659 (2018) ; DOI : 10.1039/C7TA10689K


134. Atomic-Scale Influence of Grain Boundaries on Li-ion Conduction in Li3OCl-type Solid Electrolytes for All-Solid-State Batteries

J. A. Dawson, P. Canepa, T. Famprikis, C. Masquelier & M. S. Islam

J. American Chem. Soc., 140(1), 362-368 (2018) ; DOI: 10.1021/jacs.7b10593


133. Temperature dependence of structural and transport properties for Na3V2(PO4)2F3 and Na3V2(PO4)2F2.5O0.5

T. Broux, B. Fleutot, R. David, A. Brüll, P. Veber, F. Fauth, C. Masquelier & L. Croguennec

Chem. Mater., 30(2), pp. 358-365 (2018) ; DOI: 10.1021/acs.chemmater.7b03529


132. Vanadyl-type defects in Tavorite-like NaVPO4F: from the average long range structure to local environments

E. Boivin, J. N. Chotard, T. Bamine,  D. Carlier, P. Serras, V. Palomares, T. Rojo, A. Iadecola, L. Dupont, L. Bourgeois, F. Fauth, C. Masquelier & L. Croguennec

J. Mater. Chem. A, DOI: 10.1039/c7ta08733k (2017)


131. Structural and electrochemical studies of novel Na7V4‑xAlx(P2O7)4(PO4) (x = 1, 2) high voltage electrode materials for Na batteries

V. M. Kovrugin, J. N. Chotard, R. David & C. Masquelier

J. Mater. Chem. A, DOI: 10.1039/C7TA03687F (2017)


130. Crystal structure and lithium diffusion pathways of a potential positive electrode for Lithium ion batteries: Li2VIII(PO4)(HPO4)

E. Boivin, C. Masquelier, L. Croguennec & J. N. Chotard

Inorg. Chem., DOI: 10.1021/acs.inorgchem.7b00792 (2017)


129. Understanding defects in battery materials through combined DFT/NMR studies: application to LiVPO4F

T. Bamine, F. Boucher, R. J. Messinger, E. Salager, M. Deschamps, C. Masquelier, L. Croguennec, M. Ménétrier, D. Carlier

J. Phys. Chem C, DOI: 10.1021/acs.jpcc.6b11747 (2017)


128. VIV disproportionation upon sodium extraction from Na3V2(PO4)2F3 observed by operando X-ray Absorption Spectroscopy and Solid State NMR

T. Broux, T. Bamine, L. Simonelli, L. Stievano, F. Fauth, M. Ménétrier, D. Carlier, C. Masquelier & L. Croguennec,

J. Phys. Chem C, DOI: 10.1021/acs.jpcc.6b11747 (2017)


127. Pathways to enhance lithium-ion conductivity in solid electrolytes: a mixed polyanion effect in the LISICON-type structure

Y. Deng, C. Eames, B. Fleutot, J.N. Chotard, E. Suard, C. Masquelier, S. Islam

ACS Applied Materials & Interfaces, DOI:10.1021/acsami.6b14402 (2017)


126. Oxidation under air of Tavorite LiVPO4F: influence of vanadyl-type defects on its electrochemical properties

E. Boivin, J. N. Chotard, M. Ménétrier, L. Bourgeois, T. Bamine, D. Carlier, F. Fauth, C. Masquelier, L. Croguennec

J. Phys. Chem. C, DOI: 10.1021/acs.jpcc.6b07342 (2016)


125. Strong impact of the oxygen content in Na3V2(PO4)2F3-yOy (0 <  y < 0.5) on their structural and electrochemical properties

T. Broux, T. Bamine, F. Fauth, L. Simonelli, M. Ménétrier, D. Carlier, C. Masquelier, L. Croguennec

Chem. Mater., DOI: 10.1021/acs.chemmater.6b02659 (2016)


124. Structural and Electrochemical Studies of a New Tavorite Composition: LiVPO4OH

E.  Boivin, J. N. Chotard, M. Ménétrier, L. Bourgeois, Tahya Bamine, D. Carlier, F. Fauth, E. Suard, C. Masquelier, L. Croguennec

J. Mater. Chem. A,  DOI: 10.1039/C6TA03339C (2016)


123. Spinel materials for Li-ion batteries, new insights from operando neutron and synchrotron X-Ray diffraction

M. Bianchini, F. Fauth, E. Suard, J. B.. Leriche, C. Masquelier, L. Croguennec 

Acta cryst., DOI: 10.1107/52052520615017199 (2015)


122. Discovery of a sodium-ordered form of Na3V2(PO4)3 below ambient temperature

J.N. Chotard, G. Rousse, R. David, O. Mentré, C. Masquelier,

Chem Mater., 27, 5982-5987 (2015) ; DOI: 10.1021/acs.chemmater.5b02092


121. Improving the energy density of Na3V2(PO4)3 – type positive electrodes through V / Al substitution

F. Lalère, V. Seznec, M. Courty, J. N. Chotard, C. Masquelier,

J. Mater. Chem. A, 3, 16198-16205 (2015), DOI : 10.1039/C5TA03528G


120. Structural and mechanistic insights into fast lithium-ion conduction in Li4SiO4-Li3PO4 solid electrolytes

Y. Deng, C. Eames, J. N. Chotard, F. Lalère, V. Seznec, S. Emge, O. Pecher, C. P. Grey, C. Masquelier, M. S. Islam

J. American Chem. Soc., (2015), DOI: 10.1021/jacs.5b04444 


119. Revealing Defects in Crystalline Lithium-Ion Battery Electrodes by Solid-State NMR: Applications to LiVPO4F

R. Messinger, M. Ménétrier, E. Salager, A. Boulineau, M. Duttine, D. Carlier, J. M. Ateba Mba, L. Croguennec, C. Masquelier, D. Massiot, M. Deschamps

Chem. Mater., 27, 5212-5221 (2015) ; DOI: 10.1021/acs.chemmater.5b01234


118. Singular structural and electrochemical properties in highly defective LiFePO4 powders

R. Amisse, M. Sougrati, L. Stievano, C. Davoisne, G. Dražič, R. Dominko, C. Masquelier

Chem. Mater., 27(12), 4261-4273 (2015) ; DOI: 10.1021/acs.chemmater.5b00470


117. Comprehensive investigation of the Na3V2(PO4)2F3 - NaV2(PO4)2F3 system by operando high resolution synchrotron X-ray diffraction

M. Bianchini, F. Fauth, E. Suard, C. Masquelier & L. Croguennec

Chem. Mater., 27(8), 3009-3020 (2015) ; DOI: 10.1021/acs.chemmater.5b00361


116. (NH4)0.75Fe(H2O)2[BP2O8]•0.25H2O, a Fe3+/Fe2+ mixed valence cathode material for Na battery exhibiting an helical structure

L. Tao, G. Rousse, M. T. Sougrati, J. N. Chotard, C. Masquelier

J. Phys. Chem. C, 119, 4540-4549 (2015) ; DOI: 10.1021/jp5117596 


115. Synthesis of Li2FeSiO4/Carbon Nano-Composites by Impregnation Method

S. Sun, C. M. Ghimbeu, Cathie Vix-Guterl, M.T. Sougrati, C. Masquelier, R. Janot

J. Power Sources, 284, 574-581 (2015) ; DOI: 10.1016/j.jpowsour.2015.03.028


114. Li-Rich Li1+xMn2-xO4 Spinel Electrode Materials: An Operando Neutron Diffraction study during Li+ extraction / insertion

M. Bianchini, L. Croguennec, E. Suard & C. Masquelier

J. Phys. Chem. C, 118(45), 25947-25955 (2014) ; DOI: 10.1021/jp509027g


113. One-pot synthesis of LiFePO4-carbon mesoporous composites for Li-ion batteries

S. Sun, C. Ghimbeu, R. Janot, J. M. LeMeins, A. Cassel, C. Davoisne, C. Masquelier, C. Vix-Guterl

Microporous and Mesoporous Materials, 198, 175-184 (2014) ; DOI : 10.1016/j.micromeso.2014.07.39


112. Na3V2(PO4)2F3 revisited: a high resolution diffraction study

M. Bianchini, N. Brisset, F. Fauth, F. Weill, E. Elkaim, E. Suard, C. Masquelier & L. Croguennec

Chem. Mater., 26(14), 4238-4247 (2014) ; DOI: 10.1021/cm501644g


111. Multiple phases in the ε-VPO4O - LiVPO4O - Li2VPO4O system: a combined solid state electrochemistry and diffraction structural study

M. Bianchini, J.M. Atebamba, P. Dagault, E. Bogdan, D . Carlier, E. Suard, C. Masquelier & L. Croguennec

J. Mater. Chem. A, 2, 10182-10192 (2014) ; DOI: 10.1039/C4TA01518E (2014)


110. Polymorphism in Li2MSiO4 (M = Fe, Mn): a variable temperature diffraction study

A. R. Armstrong, C. Sirisopanaporn, P. Adamson, J. Billaud, R. Dominko, C. Masquelier& P.G. Bruce

Z. Anorg. Allg. Chem., 640(6), 1043-1049 (2014) ; DOI: 10 1002/zaac.201400081(2014)


109. On the nature of phase transitions in tetragonal tungsten bronzes GdK2Nb5O15 ceramics

Y. Amira, Y. Gagou,D. Mezzane, M. Elaatmani, M. Courty, C. Masquelier, Y. Yu. Yuzyuk & M. El Marssi

J. Appl. Phys., 115, 064104 (2014)


108. Complex cation distribution in LiFeBO3

L. Tao, G. Rousse, D. Hanžel, G. Mali, R. Dominko, S. Levasseur & C. Masquelier

J. Mater. Chem A., 2(7), 2060-2070 (2014)


107. An All Solid State NASICON sodium Battery operating at 200°C

F. Lalère, J.B. Leriche, M. Courty, S. Boulineau, V. Viallet, C. Masquelier & V. Seznec

J. Power Sources, 247(1), 975-980 (2014)


106. Helicoïdal magnetic structure in LiFeAs2O7 : a neutron diffraction study

G. Rousse, C. Wurm, J. Rodriguez-Carvajal, C. Masquelier

Phys. Rev. B, 88, 214433 (2013)


105. A New Null Matrix Electrochemical Cell for Rietveld Refinements of in situ or operando neutron powder diffraction data,

M. Bianchini, J. B. Leriche, J.-L. Laborier, L. Gendrin, E. Suard, L. Croguennec & C. Masquelier,

J. Electrochem. Soc., 160(11), A2176-A2183 (2013)


104. Magnetic Structures of the Li-ion Battery Materials LiMBO3 (M = Fe, Co, Mn)

L. Tao, J. R. Neilson, B. C. Melot, T. M. McQueen, C. Masquelier, G. Rousse

Inorg. Chem., 52(20), 11966—11974 (2013)


103. Nonstochiometry in LiFe0.5Mn0.5PO4: structural and electrochemical properties

R. Amisse, S. Hamelet, D. Hanžel, R. Dominko, C. Masquelier

J. Electrochem. Soc., 160(9), A1446-A1450 (2013)


102. Towards high energy density sodium ion batteries through electrolyte optimization

A. Ponrouch, R. Dedryvère, D. Monti, A. E. Demet, J. M. Ateba Mba, L. Croguennec, C. Masquelier, P. Johansson, M. R. Palacín

Energy Environ. Sci., 6, 2361-2369 (2013)


101. Polyanionic (phosphates, silicates, sulphates,..) frameworks as electrode materials for rechargeable Li (or Na) batteries

C. Masquelier, L. Croguennec

Chem. Rev., 113(8), 6552 (2013)


100. Heterogeneous electrochemical behaviour of the lithium battery electrode LiFePO4

M. Zerrouki, G. Ouvrard, P. Soudan, B. Lestriez, C. Masquelier, M. Morcrette, S. Hamelet, J. Lesage, S. Belin, A.M. Flanck, F. Baudelet

J. Power Sources, 229, 16-21 (2013)


99. Synchrotron X-rays and neutrons as essential tools in Li battery research: examples of oxide, phosphate and silicate-based positive electrodes

C. Masquelier

European Physics Journal, 213, 213-224 (2012)


98. In-situ X-ray diffraction study of electrochemical insertion in Mg0.5Ti2(PO4)3 : an electrode material for lithium or sodium batteries.
P. Lavela, C. Vidal-Abarca, J.M. Ateba Mba, C. Masquelier, J. Tirado

J. Electrochem. Soc., 159(10), A1716-A1722 (2012)


97. Hydrothermal synthesis, silver decoration and electrochemistry of LiMPO4 (M=Fe, Mn, and Co) single-crystals

N. Recham, J. Oró-Solé, K. Djellab, M. R. Palacín, C. Masquelier, J-M. Tarascon

Solid State Ionics, 220, 47-52 (2012)


96. Lithium insertion or extraction from/into Tavorite-type LiVPO4F: an in situ X-Ray Diffraction Study

J. M. Ateba Mba, L. Croguennec, J. Barker, N.I.Basir, C. Masquelier

J. Electrochem. Soc., 159(8), A1171-A1175 (2012)


95. Synthesis and crystallographic study of homeotypic LiVPO4O and LiVPO4F

J. M. Ateba Mba, E. Suard, C. Masquelier, L. Croguennec

Chem. Mater. 24(6), 1223-1234 (2012)


94. X-ray diffraction, dielectric, conduction and Raman studies in Na0.925Bi0.075Nb0.925Mn0.075 ceramic

C. Chaker, Y. Gagou, N. Abdelmoula, J.-L. Dellis, C. Masquelier, M. El Marssi

J. Appl. Phys. 111, 04410 (2012)


93. Solid Electrolytes : Lithium ions on the fast track

C. Masquelier

Nature Materials , 10(9), 648-650 (2011)


92. Polymorphism in Li2(Fe,Mn)SiO4 : a combined diffraction and NMR study

C. Sirisopanaporn, R. Dominko, C. Masquelier, A. R. Armstrong, G. Mali, P. G. Bruce

J. Mater. Chem., DOI:10.1039/C1JM12845K (2011)


91. “Give Energy to Your Study”: Students Worldwide Gather in Europe To Design Future Materials for Energy Storage and Conversion

P. Simon, P. Knauth, J. L. Tirado, W. Wieczorek, J. Plocharski, A. Barnabé, J. M. Tarascon, C. Masquelier

J. Chem. Educ. 88, 1203-1026 ( 2011)


90. α- Na3M2(PO4)3 (M = Ti, Fe): Absolute cationic ordering in NASICON-type phases

H. Kabbour, D. Coillot, M. Colmont, C. Masquelier, O. Mentré

J. Am. Chem. Soc., 133(31), 11900-11903 (2011)


89. Electrochemical kinetic study of LiFePO4 using Cavity Microelectrode

J. Come, P.-L. Taberna, S. Hamelet, C. Masquelier,P. Simon

J. Electrochem. Soc., 158(10), 1-4 (2011)


88. Li2FeSiO4 polymorphs probed by 6Li MAS NMR and 57Fe Mössbauer spectroscopy

G.. Mali, C. Sirisopanaporn, C. Masquelier, D. Hanzel & R. Dominko

Chem. Mater., 23(11), 2735-2744 (2011)


87. Reversed Phase Composite Polymeric Electrolytes Based on Poly(oxyethylene)

J. S. Syzdek, M. Armand, P. Falkowski, M. Gizowska,M. Karzowicz, Y. Yukaszuk, M. Marcinek, A. Zalewska, M. Szafran, C. Masquelier, J. M. Tarascon, W. Wieczorek, Z. G. Zukowska

Chem. Mater., 23(7), 1785-1797 (2011)


86. Silicate cathodes for lithium batteries: alternatives to phosphates?

S. Islam, R. Dominko, C. Masquelier, C. Sirisopanaporn, R. A. Armstrong, P. G. Bruce

J. Mater. Chem., 21, 9811-9818 (2011)


85. Dependence of Li2FeSiO4 electrochemistry on structure

C. Sirisopanaporn, C. Masquelier, R.A. Armstrong, P.G. Bruce & R. Dominko

J. Am. Chem. Soc.,133, 12631265 (2011)


84. Existence of superstructures due to large amounts of Fe vacancies in LiFePO4-type framework

S. Hamelet, M. Casas-Cabanas, L. Dupont, C. Davoisne, J.M. Tarascon & C. Masquelier

Chem. Mater., 23(1), 32-38 (2011)


83. Linking Local Environments and Hyperfine Shifts: a Combined Experimental and Theoretical 31P and 7Li Solid–State NMR Study of Paramagnetic Fe(III) Phosphates and Pyrophosphates

J. Kim, D. S. Middlemiss, B. Y. X. Zhu, N. Chernova, C. Masquelier & C. P. Grey

J. Am. Chem. Soc., 132(47), 16825-16840 (2010)


82. On the origin of the electrochemical capacity in Li2Fe0.8Mn0.2SiO4

R. Dominko, C. Sirisopanaporn, C. Masquelier, D. Hanzel, I. Arcon & M. Gaberscek

J. Electrochem Soc, 157(12), A1309-A1316 (2010)


81. Crystal structure of a new polymorph of Li2FeSiO4

C. Sirisopanaporn, A. Boulineau, R. Dominko, R.D. Armstrong, P.G. Bruce & C. Masquelier

Inorg. Chem., 49(10), 7446-7451 (2010)


80. Polymorphism and structural defects in Li2FeSiO4

A. Boulineau, C. Sirisopanaporn, R. Dominko, A. R. Armstrong, P. G. Bruce& C. Masquelier

Dalton Transactions, 39(27), 6310-6316 (2010)


79. High temperature electrochemical performance of nanosized LiFePO4

F. Mestre-Aizpurua, S. Hamelet, C. Masquelier & R. Palacin

J. Power Sources, 195(19), 6897-6901 (2010)


78. An electrochemical cell for operando study of lithium batteries using synchrotron radiation

J.B. Leriche, S. Hamelet, J. Shu, M. Morcrette, C. Masquelier, G. Ouvrard, M. Zerrouki, P. Soudan, S. Belin, E. Elkaim, F. Baudelet

J. Electrochem. Soc., 157(5), A606-A610 (2010)


77. Crystal structures and sodium/silver distributions within the ionic conductors Na5Ag2Fe3(As2O7)4 and Na2Ag5Fe3(P2O7)4

Eric Quarez, Olivier Mentré, K. Djellab & C. Masquelier

New J. Chem., 34, 287-293 (2010)


76. Lithium insertion mechanism in crystalline and amorphous FePO4.nH2O

C. Delacourt, P. Poizot, D. Bonnin & C. Masquelier

J. Electrochem. Soc., 156(7), A595-A605 (2009)


75. The effects of moderate thermal treatments under air on LiFePO4-based nanopowders

S. Hamelet, P. Gibot, M. Casas Cabanas, D. Bonnin, C. Grey, J. Cabana, J. B. Leriche, J. Rodriguez Carvajal, M. Courty, S. Levasseur, P. Carlach, M. Van Thournout, J. M. Tarascon & C. Masquelier

J. Mater. Chem., 19, 3979-3991 (2009)


74. Comparative studies on the phase stability, electronic structure and topology of the charge density in the Li3XO4 (X = P, As, V) lithium orthosalt polymorphs

C. Frayret, C. Masquelier, A. Villesuzanne, M. Morcrette & J.M. Tarascon

Chem. Mater., 21(9), 1861-1874 (2009)


73. Crystal structures of new silver ion conductors Ag7Fe3(X2O7)4 (X = P, As)

E. Quarez, O. Mentré, Y. Oumellal & C. Masquelier

New J. Chem., 33, 998-1005 (2009)


72. Better electrode materials for Li-based batteries via diversified chemical approaches
N. Recham, M. Armand, R. Janot, C. Masquelier, L. Dupont, J.-M. Tarascon

Zeitschrift für anorganische und allgemeine Chemie, 634, 11 (2008)


71. Room-temperature single-phase Li insertion/extraction in nanoscale LixFePO4

P. Gibot, M. Casas-Cabanas, L. Laffont, S. Levasseur, P. Carlach, S. Hamelet, J-M. Tarascon & C. Masquelier,

Nature Materials, 7, 741-747 (2008)


70. Doping effects on the phase transition of LiMn2O4 by anelastic spectroscopy and differential scanning calorimetry
A. Paolone, R. Cantelli, B. Scrosati, P. Reale, M. Ferretti & C. Masquelier

Mater. Sc & Engineering, A, 442 (1-2), 220-223, (2006)


69. Comparative study of the phase transition of Li1+xMn2−xO4 by anelastic spectroscopy and differential scanning calorimetry

A. Paolone, R. Cantellia, B. Scrosati, P. Reale, M. Ferretti and C. Masquelier

Electrochem. Comm. 8 (1), 113-117 (2006)


68. Study of the LiFePO4 / FePO4 two-phase system by high-resolution electron energy loss spectroscopy

L. Laffont, C. Delacourt, P. Gibot, M. Y. Wu, P. Kooyman, C. Masquelier & J.M. Tarascon
Chem. Mater., 18 (23): 5520-5529 (2006)


67. Size effects on carbon-free LiFePO4 powders: the key for superior energy density

C. Delacourt, P. Poizot & C. Masquelier

Electrochem. Solid State Lett. 9, A352 (2006)


66. Electrochemical and electrical properties of Nb- and/or C-containing LiMPO4 composites (M = Fe, Mn)

C. Delacourt, C. Wurm, L. Laffont, J.-B. Leriche & C. Masquelier

Solid State Ionics, 177(3-4), 333-341 (2006)


65. Energetics of LiFePO4 and polymorphs of its delithiated form, FePO4

R. G. Lyer, C. Delacourt, C. Masquelier, J. M. Tarascon &  A. Navrotsky

Electrochem. Solid State Lett.  9(2), A46-A48 (2006)


64. Crystal chemistry of the olivine-type LixFePO4 system (0 < x < 1) between 25 and 370°C

Charles Delacourt, Juan Rodriguez-Carvajal, Bernd Schmitt, Jean-Marie Tarascon & Christian Masquelier

Solid State Sciences, 7, 1506-1516 (2005)


63. Synthesis, Phase Stability, and Electrochemically Driven Transformations in the LiCuO2-Li2CuO2 System

A. S. Prakash, D. Larcher, M. Morcrette, M. S. Hegde, J-B. Leriche, & C. Masquelier

Chem. Mater., 17(17), 4406-4415 (2005)


62. The existence of a temperature-driven solid solution for 0 < x < 1 in LixFePO4

C. Delacourt, P. Poizot, J.M. Tarascon & C. Masquelier

Nature Materials, 4, 254–260 (2005)


61. Towards the understanding of electrical limitations (electronic, ionic) in LiMPO4 (M = Fe, Mn) electrode materials

C. Delacourt, L. Laffont, R. Bouchet, C. Wurm, J.-B. Leriche, M Morcrette, J.-M. Tarascon & C. Masquelier

J . Electrochem. Soc., 152 (5) A913-A921 (2005)


60. Stabilization of an orthorhombic phase in LiMn2O4 by means of high pressure
A. Paolone, A. Sacchetti, P. Postorino, R. Cantelli, A. Congeduti, G. Rousse & C. Masquelier

Solid State Ionics, 176, 5-6, 635-639 (2005)


59. Various strategies to tune the ionic/electronic properties of electrode materials,

J. M. Tarascon, C. Delacourt, A. S. Prakash, M. Morcrette, M. S. Hegde, C. Wurm & C. Masquelier

J. Chem. Soc., Dalton Trans 2988-2994 (2004)


58. Low temperature preparation of optimized phosphates for Li-battery applications
C. Delacourt, C. Wurm, P. Reale, M. Morcrette & C. Masquelier

Solid State Ionics, 173, 1-4, 113-118 (2004)


57. Structural and Electrochemical Studies of orthorhombic Li2+xTiFe(PO4)3 and Li2+xTiCr(PO4)3

S. Patoux, G. Rousse, J.B. Leriche & C. Masquelier

Solid State Sciences, 6(10), 1113-1120 (2004)


56. MicroRaman spectroscopy on LiMn2O: warnings on laser-induced thermal decomposition
A. Paolone, A. Sacchetti, T. Corridoni, P. Postorino, R. Cantelli, G. Rousse & C. Masquelier

Solid State Ionics, 170, 1-2, 135-138 (2004)

55. Disproportionation of stoichiometric LiMn2O4 on annealing in oxygen

P. Strobel, G. Rousse, A. Ibarra Palos & C. Masquelier

J. Solid State Chem., 1-5, 177 (2004)


54. A one step low-temperature route for the preparation of electrochemically active LiMnPO4 powders

C. Delacourt, P. Poizot, M. Morcrette, J. M. Tarascon & C. Masquelier

Chem. Mater., 16(1), 93-99 (2004)


53. Synthesis and thermal behaviour of crystalline Hydrated Iron (III) Phosphates of interest as Positive Electrodes in Li Batteries

P. Reale, B. Scrosati, C. Delacourt, C. Wurm, M. Morcrette and C. Masquelier

Chem. Mater., 15(26), 5051-5058 (2003)


52. Magnetic structures of the triphylite LiFePO4 and of its delithiated form FePO4

G. Rousse, J. Rodriguez-Carvajal, S. Gwizdala, S. Patoux and C. Masquelier

Chem. Mater, 15(21), 4082-4090 (2003)


51. Structural and electrochemical studies of rhombohedral Na2TiM(PO4)3 and Li1.6Na0.4TiM(PO4)3 (M = Fe, Cr) phosphates

S. Patoux, G. Rousse, J.B. Leriche and C. Masquelier

Chem. Mater, 15(10), 2084-2093 (2003)


50. Evidence of a splitting of the Mn-O distance and of large lattice disorder in the charge ordered phase of LiMn2O4 obtained by EXAFS

A. Paolone, C. Castellano, R. Cantelli, G. Rousse and C. Masquelier

Phys. Rev. B, 68, 014108 (2003)


49. Development of potentiometric ion sensors based on insertion materials as sensitive elements

N. Le Poul, E. Baudrin, M. Morcrette, S. Gwizdala, C. Masquelier and J.M. Tarascon

Solid State Ionics, 8877 (2003) 1-10


48. In situ X-ray diffraction during lithium extraction from rhombohedral and monoclinic Li3V2(PO4)3

M. Morcrette, J.B. Leriche, S. Patoux, C. Wurm and C. Masquelier,

Elec. And Solid State Letters, 6(5) A80-A84 (2003)


47. A comparative structural and electrochemical study of monoclinic Li3Fe2(PO4)3 and Li3V2(PO4)3

S. Patoux, C. Wurm, G. Rousse, M. Morcrette and C. Masquelier,

J. Power Sources, 119-121, 278-284 (2003)


46. Effect of particle size on lithium intercalation into a-Fe2O3

D. Larcher, C. Masquelier, D. Bonnin, Y. Chabre, V. Masson, J. B. Leriche and J.M. Tarascon,

J . Electrochem. Soc., 150(1) A133-139 (2003)


45. The charge order transition and elastic / anelastic properties of LiMn2O4
A. Paolone, R. Cantelli, G. Rousse, C. Masquelier.
J. Physics Cond. Matter., 15, 3, 457-465 (2003)


44 Lithium insertion into titanium oxides, phosphates, silicates and sulfates

S. Patoux and C. Masquelier,

Chem. Mater.,14(12), 5057-5058 (2002)


43. In situ X-ray diffraction techniques as a powerful tool to improve battery electrode materials

M. Morcrette, Y. Chabre, G. Vaughan, G. Amatucci, J.B. Leriche, S. Patoux, C. Masquelier and J.M. Tarascon,

Electrochimica Acta, 47, 3137-3149 (2002)


42. Lithium insertion/extraction into/from LiMX2O7 compositions (M = Fe, V) prepared via a solution method

C. Wurm, M. Morcrette, G. Rousse, L. Dupont and C. Masquelier,

Chem. Mater14(7), 2701-2710 (2002)


41. FePO4 . nH2Oand Fe4(P2O7)3 . nH2O : hydrated iron phosphates as 3 V positive electrodes in rechargeable lithium batteries

C. Masquelier, P. Reale, C. Wurm, M. Morcrette, L. Dupont and D. Larcher,

J . Electrochem. Soc. 149(8), A1037-A1044 (2002)


40. Chemical and electrochemical insertion of lithium in two allotropic varieties of NbPO5

S. Patoux and C. Masquelier,

Chem. Mater.14(5), 2334-2341 (2002)


39. A neutron diffraction study of the antiferromagnetic diphosphate LiFeP2O7

G. Rousse, C. Wurm, C. Masquelier andJ. Rodríguez-Carvajal,

Solid State Sciences, 4, 973-978 (2002)


38. A reversible lithium intercalation process in an ReO3-type structure : PNb9O25

S. Patoux, M. Dollé, G. Rousse and C. Masquelier,

J. Electrochem. Soc. 149(4), A391-A400 (2002)


37. On the way to the optimization of Li3Fe2(PO4)3 positive electrode materials

M. Morcrette, C. Wurm and C. Masquelier,

Solid State Sciences, 4, 239-246 (2002)


36. Magnetic structural studies of the two polymorphs of Li3Fe2(PO4)3 : analysis of the magnetic ground state from super-superexchange interactions

G. Rousse, J. Rodríguez-Carvajal, C. Wurm and C. Masquelier,

Chem. Mater., 13, 4527-4536 (2001)


35. Investigation of Positive Electrode Materials for Lithium Batteries by Means of X-ray and Neutron Diffraction

C. Masquelier, M. Morcrette and G. Rousse,

ESRF NewsLetter, pp 22-24, June 2001


34. On the role of defects in decreasing the extra 3.3/3.95 and 4.5 V redox steps in Li-Mn-O spinels

M. R. Palacin, G. Rousse, M. Morcrette, L. Dupont, C. Masquelier, Y. Chabre, M. Hervieu and J. M. Tarascon,

J. Power Sources, 4180, 1-4 (2001)


33. Crystal Structure of a new vanadium(IV) diphosphate : VP2O7, prepared by lithium extraction from LiVP2O7

G. Rousse, C. Wurm, M. Morcrette, J. Rodriguez-Carvajal, J. Gaubicher and C. Masquelier,

Int. J. Inorg. Mater., 3, 881-887 (2001)


32. A powder neutron diffraction investigation of the two rhombohedral NASICON analogs : g-Na3Fe2(PO4)3 and Li3Fe2(PO4)3

C. Masquelier, Calin Wurm, J. Rodríguez-Carvajal, J. Gaubicher, and L. Nazar,

Chem. Mater., 12(2), 525-532 (2000)


31. On the Origin of the 3.3V and 4.5V steps observed in LiMn2O4 spinels

M. R. Palacin, Y. Chabre, L. Dupont, M. Hervieu, P. Strobel, G. Rousse, C. Masquelier, M. Anne, G. Amatucci and J. M. Tarascon,

J. Electrochem. Soc. 147 (3) 845-853 (2000).


30. TEM studies: the key for understanding the origin of the 3.3V and 4.5V steps in LiMn2O4 based spinels

L. Dupont, M. Hervieu, G. Rousse, C. Masquelier, M.R. Palacín, Y. Chabre and J.M. Tarascon,

J. Solid State Chem. 155, 394-408 (2000).


29. Rhombohedral form of Li3V2(PO4)3 as a cathode in Li-ion batteries

J. Gaubicher, C. Wurm, G. Goward, C. Masquelier and L. Nazar,

Chem. Mater. 12, 3240-3242 (2000).


28. Solubility range and ionic conductivity of large trivalent ion doped Na1+xMxZr2-xP3O12 (M : In, Yb, Er, Y, Dy, Tb, Gd) solid electrolytes
Y. Miyajima, T. Miyoshi, J. Tamaki, M. Tabuchi, C. Masquelier
Solid State Ionics, 124(3-4), 201-211 (1999)


27. Cubic to orthorhombic transition in the stoichiometric spinel LiMn2O4.

G. Rousse, C. Masquelier, J. Rodriguez-Carvajal and M. Hervieu,

Elec. & Solid State Letters, 2 (1), 6-8 (1999).


26. Preparation of LiCoO2 and LiCo1-xFexO2 using hydrothermal reactions.

M. Tabuchi, K. Ado, H. Kobayashi, H. Sakaebe, H. Kageyama, C. Masquelier, M. Yonemura, A. Hirano and R. Kanno,

Journal of Materials Chemistry, 9, 199-204, (1999).


25. Infrared spectroscopy investigation of the charge ordering transition in LiMn2O4

A. Paolone, P. Roy, G. Rousse, C. Masquelier, J. Rodriguez-Carvajal,

Solid State Comm., 111, 453-458 (1999)


24. The relationships between phases and structures of lithium manganese spinels

R. Kanno, A. Kondo, M. Yonemura, R. Gover, Y. Kawamoto, M. Tabuchi, T. Kamiyama, C. Masquelier, G. Rousse,

Journal of Power Sources, 81-82, 542-546 (1999).


23. X-Ray study of the spinel LiMn2O4 at low temperatures

G. Rousse, C. Masquelier, J. Rodriguez-Carvajal, E. Elkaim, and J. P. Lauriat, J. L. Martinez

Chem. Mater., 11(12), 3629-3635 (1999)


22. New cathode materials for rechargeable lithium batteries : the 3-D framework structures Li3Fe2(XO4)3.

C. Masquelier, A. K. Padhi, K. S. Nanjundaswamy and J. B. Goodenough,

J. Solid State Chem., 135, 228-234 (1998).


21. Synthesis of LiMnO2 with NaMnO2 type structure by a mixed-alkaline hydrothermal reaction.

M. Tabuchi, K. Ado, H. Kobayashi, H. Kageyama, C. Masquelier, A. Kondo and R. Kanno,

J. Electrochem. Soc. 145 [4], L49-L52 (1998).


20. Effect of cation arrangement on the magnetic properties of lithium ferrites (LiFeO2) prepared by hydrothermal reaction and post-annealing method.

M. Tabuchi, S. Tsutsui, C. Masquelier, R. Kanno, K. Ado, I. Matsubara, S. Nasu and H. Kageyama,

J. Solid State Chem. 140, 159-167 (1998).


19. Magnetic properties of metastable lithium iron oxides obtained by solvothermal / hydrothermal reaction

M. Tabuchi, H. Kobayashi, I. Matsubara, H. Kageyama, S. Tsutsui, S. Nasu, C. Masquelier, A. Hirano and R. Kanno,

J. Solid State Chem. 141, 554-561 (1998).


18. Electronic crystallization in a lithium battery material: columnar ordering of electrons and holes in the spinel LiMn2O4

J. Rodriguez-Carvajal, G. Rousse, C. Masquelier and M. Hervieu,

Phys. Rev. Letters, 81, 1460, Nov. 23 (1998)


17. Effect of structure on the Fe3+/Fe2+ redox couple in iron phosphates

A.K. Padhi, K. S. Nanjundaswamy, C. Masquelier, S. Okada, and J. B. Goodenough,

J. Electrochem. Soc. 144(5), 1609-1614 (1997)


16. Mapping of transition-metal redox energies in phosphates with NASICON structure by lithium intercalation

A.K. Padhi, K. S. Nanjundaswamy, C. Masquelier, J. B. Goodenough,

J. Electrochem. Soc. 144(8), 2581-2588 (1997)


15. Characterization of Li1-dMn2-2dO4 defect spinel materials by their phase transition, magnetic and electrochemical properties

M. Tabuchi, C. Masquelier, H. Kobayashi, R. Kanno, Y. Kobayashi, Y. Maki, H. Kageyama and O. Nakamura,

J. Power Sources, 68, 623-628 (1997)


14. Electrochemical and magnetic properties of lithium manganese oxide spinels prepared by oxidation at low temperature of hydrothermally obtained LiMnO2

M. Tabuchi, K. Ado, C. Masquelier, I. Matsubara, H. Kageyama, R. Kanno, H. Kobayashi, and O. Nakamura,

Solid State Ionics, 89, 53-63 (1996)


13. Chemical and magnetic characterization of spinel materials in the LiMn2O4 - Li2Mn4O9 - Li4Mn5O12 system

C. Masquelier, M. Tabuchi, K. Ado, R. Kanno, Y. Kobayashi, Y. Maki, O. Nakamura, and J. B. Goodenough,

J. Solid State Chem. 123, 255-266 (1996)


12. Li+/Na+ exchange from NaFeO2 using hydrothermal reaction

M. Tabuchi, C. Masquelier, T. Takeuchi, I. Matsubara, T. Shirane, R. Kanno, H. Sakaebe, and O. Nakamura,

Solid State Ionics, 90, 129-132 (1996)


11. Characteristics of 3D framework cathodes with (XO4)n- polyanions

S. Okada, Y. Sakurai, J. Yamaki, K. S. Nanjundaswamy, A. K. Padhi, C. Masquelier and J. B. Goodenough,

Prog. in Lithium Ion Batteries, Edit. M. Yoshio, M. Thackeray and A. Kozawa, (1996)


10. Crystal structure of Na7Fe4(AsO4)6 and Na3Al2(AsO4)3 ; two sodium ion conductors structurally related to II-Na3Fe2(AsO4)3

C. Masquelier, F. d'Yvoire and G. Collin,

J. Solid State Chem. 118, 33-42 (1995)


9. Effect of content of BaTiO3 surface cubic layer on the ionic conductivity enhance-ment in composite solid electrolytes

T. Takeuchi, K. Ado, Y. Saito, M. Tabuchi, C. Masquelier and O. Nakamura,

Solid State Ionics, 79, 325-330 (1995)


8. Preparation of AFeO2 (A = Li, Na) by hydrothermal method

M. Tabuchi, K. Ado, H. Sakaebe, C. Masquelier, H. Kageyama and O. Nakamura,

Solid State Ionics, 79, 220-226 (1995)


7. Chemistry and structure analysis in the Li4+xBxSi1-xO4 solid solution

C. Masquelier, H. Kageyama, T. Takeuchi, Y. Saito and O. Nakamura,

J. Power Sources, 54, 448-451 (1995)


6. Influence of the preparation process on the cation transport properties of Li4+xMxSi1-xO4 (M = B, Al) solid electrolytes

C. Masquelier, M. Tabuchi, T. Takeuchi, W. Soizumi, H. Kageyama and O. Nakamura,

Solid State Ionics, 79, 98-105 (1995)


5. A new family of sodium ion conductors, the diphosphates and diarsenates Na7M3(X2O7)4 (M=Al, Ga ,Cr ,Fe, X=P, As)

C. Masquelier, F. d'Yvoire, E. Bretey, P. Berthet and C. Peytour,

Solid State Ionics, 67, 183-189 (1994)


4. Analysis of double layered structure of submicron BaTiO3 grains using equivalent circuit model

T. Takeuchi, K. Ado, T. Asai, H. Kageyama, K. Honjo, Y. Saito, C. Masquelier and O. Nakamura,

J. Ceram. Soc. Japan, International Edition, 102, No. 12, 1178-1181 (1994)


3. Thickness of the cubic surface phase on baryum titanate fine particles

T. Takeuchi, K. Ado, T. Asai, H. Kageyama, Y. Saito, C. Masquelier and O. Nakamura,

J. American Ceramic Society, 77, 1665-1668 (1994)


2. Crystal structure of the sodium ion conductor α-Na7Fe3(P2O7)4 : evidence of a long-range ordering of the Na+Ions

C. Masquelier, F. d'Yvoire and N. Rodier,

J. Solid State Chem. 95, 156-167 (1991)


1. Structure of the sodium ion conductor Na7Fe3(As2O7)4

C. Masquelier, F. d'Yvoire and N. Rodier,

Acta Cryst. C 46, 1584-1587 (1990)

Credit : Utkarsh VIJAY, PhD candidate @ LRCS


July 3-5, 2024 : The 20-years Anniversary of the MESC+ ERASMUS MUNDUS Master Course gathers >180 people in Amiens. Great Celebaration with bright ALumnis from all over the world.


June 4-6, 2024 : The ALISTORE ERI European Research Network celebtrates its 20th Anniversary in Chalmers University, Sweden. 


February 13, 2024: Dhanush SHANBHAG is now a Doctor of Université de Picardie Jules Verne, Amiens, FRANCE, after his superb work on Argyrodite-type ionic conductors for All Solid State Batteries.  Very fruitful collaboration with V. VIALLET from LRCS Amiens and UMICORE, Belgium. Four Patents are filled.  


January 16, 2024: Yearly Review Meeting in Paris of the "PEPR Batteries" project, a 50 MEuros French initiative on disruptive Battery Technologies and Chemistries, coordinated by CNRS (Patrice SIMON & Mathieu MORCRETTE) and CEA (Hélène BURLET). 


December 14 & 15, 2023: The traditional "Journées Scientifiques" of the LRCS, with 47 talks given by PhD candidates and Post-Docs. Lots of exciting science + a superb and friendly lunch with local dishes from 22 nationalities !!!!


December 6 & 7, 2023: 37th Bi-Annual Meeting of the ALISTORE European Network. Superb organization by Sergio BRUTTI and his team in Universita Roma La Sapienza. 


December 4, 2023: Eunike MAHAYONI is now a Doctor of Université de Picardie Jules Verne, Amiens, FRANCE, after her superb work on NZSP Nasicons solid electrolytes, in the frame of the Na-Master ANR Project. Fruitful collaboration with P. CANEPA and S. ADAMS from NUS Singapore, O. GUILLON and Q. MA from Jülich, V. SEZNEC and J.N. CHOTARD from LRCS Amiens. 


November 1, 2023: Gave a talk at the 14th ABAA Conference in Ho Chi Minh City, VIETNAM. On NASICON Cathodes for Na-Ion Batteries. Solid Electrolytes. Big Crowd. Superb organisation by Khalil AMINE and his team


October 18, 2023: Paper on ZrO2-free NASICON solid electrolytes, published in J. Mater. Chem. A. with Eunike MAHAYONI as second author. Collaborative work with P. CANEPA and his team from NUS SIngapore.


October 17, 2023: Briseis MERCADIER is now a Doctor of Sorbonne Université, after her superb work on BaSnF4-type solid electrolytes.  Collaboration with D. DAMBOURNET from PHENIX Lab. in Paris, B. MORGAN from Univ. of Bath in UK, ICMCB Bordeaux. 


October 16, 2023: Paper on BaSnF4 lone pair published in JACS with Briseis MERCADIER as first author!!


October 12, 2023: Online Talk at the Solid State Chemistry Division of the Société Chimique de France.


October 5-6, 2023: attending the RS2E bi-annual Meeting in University of Caen @CRISMAT Laboratory.


May 17, 2023: Kick Off of the LIMASSE Project on Solid State Batteries, a "target" action of the PEPR on Batteries. 


May 10, 2023: Paper on Na3V2(PO4)2(F,O)3 with Chloé PABLOS as first author, accepted in Chem. Mater.


March 21, 2023: Attending the RS2E bi-annual Meeting in Bordeaux, @ICMCB Institute


March 21, 2023:  Paper on the sodium-rich NASICON cathode Na4MnV(PO4)3, by the great Sunkyu PARK, accepted for publication in Chem. Mater.,


March 15-17 2023: Selection of Class#19 of MESC+ Master Course, in WUT Warsaw, among
> 400 applicants    


March 6-9 2023: Gave a talk at the IBA Conference in Austin, USA, on Argyrodite Solid Electrolytes. Superb organisation by Manthiram and his team.


January 11-13, 2023: Kickoff Meeting for Cohort#2 of DESTINY Marie Curie PhD program. In beautiful Bohinj, SLOVENIA. 


October 13, 2022: Attending the RS2E bi-annual Meeting in Montpellier @ICG Institute


October 5, 2022: Gave a talk at IBA Conference in Slovenia on Na3PS4 Solid Electrolyte


September 26, 2022: Gave a talk at Na-Ion Symposium in Berlin, on NASICON electrodes


September 19, 2022 : Giving a talk on NASICON electrodes at the E-MRS Meeting in Warsaw


July 12 2022 : Sunkyu PARK is now a "Docteur de l'Université de Picardie Jules Verne", Amiens, FRANCE. For his great work on NASICON electrodes for Na Batteries, funded by TIAMAT and ANRT, in strong collaboration with ICMCB Bordeaux and NUS Singapore. Thank you SUNKYU !!


December 29, 2021 : Paper on the structure of Na2V2(PO4)3, solved by Sunkyu PARK, published in Chem. Mater


December 17, 2021 : Cédric BARCHA is now a "Docteur de l'Université de Picardie Jules Verne", Amiens, FRANCE. For his great work on interface stabilities in solid state batteries, in collaboration with RENAULT through a CIFRE funding. Thank you CEDRIC !!


December 14, 2021 Kickoff of the DESTINY PhD Cofund Marie Curie Project (50 PhDs....) in Amiens as a joint event with the ALISTORE bi-annual Meeting


December 2, 2021 : Na2V2(PO4)3 spotted by Ziliang WANG and P. CANEPA'S team (NUS Singapore) through computational methods, published in J. Mater. Chem. A


June 19, 2021 : One more great paper from Theodosios FAMPRIKIS on Na3PS4, accepted in Chem. Mater


June 15, 2021 : First paper from Sunkyu PARK on his PhD work, on NaxFeV(PO4)3, accepted in Chem. Mater.


March 29 & 30, 2021: Oral interviews for the Marie Curie PhD CO-FUND project DESTINY. 29 topics on "batteries" in Europe. 


November 10, 2020: Theodosios FAMPRIKIS is now a "Docteur de l'Université de Picardie Jules Verne", Amiens, FRANCE. For his great work on solid electrolytes, in particular Na3PS4, in collaboration with Prof. S. ISLAM @ Univ. Bath, through an ALISTORE funding.  Thanks you THEO !!


September 24, 2020 : Paper accepted in J. Mater. Chem. A  on Na7V3(P2O7)4, with Vadim KOVRUGIN as main author.


September 14, 2020 : Paper accepted in J. Amer. Chem. Soc. on Na3PS4 and pressure effects on solid electrolytes, with Theodiosios FAMPRIKIS as main author.


August 30, 2020 : Paper accepted in J. Power Sources, a review on Na-Batteries, with Montse CASAS-CABANAS as leader of a great team of contributors.


July 13, 2020 : 30 PhD topics received for the first Pre-Call of the MSCA PhD Cofund project DESTINY. An exciting adventure begins.


June 8, 2020 : Paper accepted in J. Power Sources on Na-containing Antiperovskites, with Ernest AHIAVI and Theo FAMPRIKIS as main contributors.


May 29, 2020 : Omer Ulas KUDU is now a "Docteur de L'Université de Picardie Jules Verne", Amiens, FRANCE. For his great work on solid electrolytes within the Li2S-P2S5 system, in collaboration with SOLVAY.  Thank you ULAS !!


April 1, 2020 : Official start of our Bilateral ANR-NSG, i.e. France-Singapore, project on Na-containing solid electrolytes, with Pieremanuele CANEPA, Stefan ADAMS and Tony CHEETHAM as collaborators from NUS, Jean-Noël CHOTARD, Vincent SEZNEC and Christine FRAYRET as co-workers from LRCS.


February 3, 2020 : The EU informs me that they accepted our 8 Million Euros Marie Curie COFUND project, DESTINY. 50 PhD projects to be granted to talented students witin the frames of the ALISTORE Network and the BATTERY 2030+ Initiative. 


February 6 & 7, 2020 : The National Committee on Materials Science (CNU, Section 33) gathers in Montpellier to examine the files of candidates for "Qualifications" for Assistant-Professor and Full Professor positions in France.  


January 8, 2020 : Congrats to Theodosios FAMPRIKIS, recipient of the Ludo Frevel Crystallography Scholarship Award from ICDD. 


December 12, 2019 : Long NGUYEN defended his PhD Thesis in Université de Bordeaux, FRANCE. Wonderful work. He will join Prof. Shirley MENG's group in UCSD, as a PDRA, starting March 2010. 


December 10-11, 2019 : The 27th ALISTORE ERI Meeting was held in Barcelona, hosted by M.R. PALACIN. A special tribute to the Nobel Prize in Chemistry was given by Mike THACKERAY. 


November 21, 2019 : Mathieu MORCRETTE, the head of LRCS, receives the "Médaille de Cristal" of the CNRS, a prestigious recognition for his achievements in Amiens


October 30, 2019 : The Crystal structure of a new polymorph of Na3PS4, discovered by Theo FAMPRIKIS, is published in ACS Materials Letters.


October 15-17, 2019 :  Around 120 people gather in Amiens for the RS2E Meeting. Lots of excellent science on many fronts of advanced battery and supercapacitor research.


Sept. 26, 2019 : Submission of the DESTINY project under the Marie Curie COFUND Scheme : 40 partners from 12 countries, 50 PhD thesis to be funded.... Results in February 2020 !!


June 19-20, 2019 : 28th Meeting of the ALISTORE-ERI in Vitoria (SPAIN) in the premises of our Partner CIC-Energigune


March 25-27, 2019 : Meeting of the MESC+ Consortium in Toulouse, FRANCE, to select 20 students for EMJMD Scholarships, among many applicants (>250).


March 19-20, 2019 : Bi-annual Meeting of the RS2E Network, Lille, FRANCE.


March 4-8, 2019 : IBA International Meeting in UCSD, La Jolla, USA. Organized by Prof. Shirley MENG


October 17-18, 2018 :  RS2E bi-annual Meeting (120 participants) in ICG Montpellier


October 1st, 2018 :  Ulas KUDU's review paper on Li2S-P2S Solid Electrolytes accepted in J. Power Sources 


September 27th, 2018 : Big proposal submitted for the Marie Curie COFUND action; DESTINY gathers 40 european partners for 53 PhD thesis proposed.


July 26th, 2018 : Fan CHEN's first paper accepted in SMALL Methods, on Na4MnV(PO4)3


July 24th, 2018 : Thibaut BROUX's paper accepted in SMALL Methods, on high rate Na3V2(PO4)2F3


June 26th, 2018 : MESC+ is granted as an EMJMD ERASMUS MUNDUS Master Course for 5 more years, with partners in Spain, Slovenia, Poland, France, USA and Australia


April 25th, 2018: Attending the 34th PSI Electrochemical Symposium in Villigen, SWITZERLAND. Talk on operando investigations of Li and Na battery materials.


April 24th 2018: Mattéo BIANCHINI's paper accepted in J. Mater Chem. A. on Na+ - Ag+ ion exchange in Na3V2(PO4)2F3 


Jan. 19th, 2018: Simon MALIFARGE defends his PhD Thesis in UPJV Amiens


Dec. 12th, 2017: ALISTORE Meeting in Amiens, FRANCE. New Direction elected with P. JOHANSSON, R. DOMINKO and myself as Directors. Thanks A LOT to R. PALACIN and P. SIMON for their leadership during the previous term.


Dec. 11th, 2017: Thibault BROUX's paper accepted in Chem. Mater. on transpot properties of Na3V2(PO4)2F3


Nov. 29th, 2017: Attending the 4th International Na-ion Battery Conference in Tokyo, JAPAN. 


Nov. 24th, 2017: Edouard BOIVIN defends hs PhD thesis in UPJV Amiens


Sept. 28th, 2017: Application for a COFUND Programme (Marie Curie Action)


May 30th, 2017: Attending the 8th ICE Conference in Nagoya, JAPAN 


February 15th, 2017: New Application of MESC Consortium for ERASMUS + EMJMD.


February 5th, 2017: the LRCS moves to its new building, the HUB of the RS2E French Network on Electrochemical Energy Storage.


February 5th, 2017: Paper #2 of Thibault BROUX, on VIV disproportionation in NVPF upon charge, accepted in ACS J. Phys. Chem. C


February 1st, 2017: Paper #2 of Yue DENG, on mixed anion effect in solid electrolytes, accepted in ACS Applied Materials & Interfaces


October 24th, 2016 : Paper #2 of Edouard BOIVIN, on LiVPO4(F,O) accepted in J. Phys. Chem. C.


October 6th, 2016 : Paper #1 of Thibault BROUX on Na3V2(PO4)2F3 accepted in Chem. Mater.


October 5th, 2016 : The Nobel Prize for Chesmistry is attributed to Jean-Pierre SAUVAGE from Strasbourg.


June 28-29, 2016 : ERAMUS + Meeting in Brussels on "Mastering Joint Excellence under ERASMUS MUNDUS" 


June 14-18, 2016 : IMLB 2016 in Chicago, 1800 attendees......


April 12-15, 2016 : Proposals Subcommittees and Scientific Council at ILL, Grenoble, FRANCE


March. 22, 2016 : Talk at IBA Conference, Nantes, France


Feb. 18, 2016 : Application of M.E.S.C. for ERASMUS + re-accreditation ......


Dec. 5, 2015 : Interview of Mathieu MORCRETTE, Director of LRCS, in "Agir en Picardie".



Nov. 23-25, 2015 :CNRS-sponsored ANF Chimie du Solide, organized in Caen, France.


Nov. 9, 2015 : PhD Defense of Fabien LALERE in UPJV Amiens 


Oct. 23, 2015 : PhD Defense of Matteo BIANCHINI in UPJV Amiens 


Sept. 15, 2015 : Graduation Ceremony in Amiens of Class#10 of M.E.S.C. Master Course.


Sept. 2, 2015 : invited Talk at European Conference on Neutron Scattering, Zaragoza, Spain


August 7, 2015 : New Crystal Structure of Na3V2(PO4)3 published in Chem. Mater.


July 1, 2015 : Yue DENG's first paper on Li4SiO4-Li3PO4 is published in JACS.


July 1, 2015 : Invited talk at ICMAT Singapore on highly defective LiFePO4 powders.


June 16, 2015 : Fabien LALERE gives a talk in SSI Conference, Keyston, USA


June 4, 2015 : Matteo BIANCHINI is the ECS Battery Student Award winner for 2015


June 1, 2015 : Robin AMISSE's paper on highly defective LiFePO4 accepted in Chemistry of Materials 


Nov 24, 2014 : the www site is launched. There is in particular a very convenient Job section.


July 23, 2014 : Visit the www site of Nature related to CRYSTALLOGRAPHY, MILESTONES


July 11, 2014 : HDR Defense of Joël GAUBICHER, IMN Nantes, France


June 15-18 : EPDIC Conference in Aarhus, Denmark.


June 7-12, 2014 : IMLB conference, Como, Italy


May 6, 2014 : Comité de Sélection, Poste 33MCF0269, Amiens


April 16th, 2014 : Conseil Académique à l'UPJV Amiens.


April 2-4, 2014 : Power our Future at CIC Energigune, SPAIN


March 18 & 19, 2014 : ILL Subcommittees for experiments, Grenoble, FRANCE 


March 3-7, 2014 : IBA Meeting in Brisbane, Australia


Feb. 24-25, 2014 : Meeting of the French RS2E in Lyon, FRANCE.


Feb. 11-13, 2014 : Meeting of the MESC Consortium in Marseille for the Selection of CLass#11 (2014-2016)


February 7, 2014 : All Solid State Battery Meeting of the RS2E.


February 7, 2014 : Na-ion Group Meeting of the RS2E


January 24, 2014 : Li-Ion Group Meeting of the RS2E in Collège de France, Paris


January  23, 2014 : Prof. J.M. TARASCON gives his Inaugural Lecture at College de France, Paris

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