Christian MASQUELIER @ LRCS - Amiens
Christian MASQUELIER          @ LRCS - Amiens

Publications in peer-reviewed Journals

Note : You may request a pdf reprint of some of these publications, by sending an e-mel to


130. Crystal structure and lithium diffusion pathways of a potential positive electrode for Lithium ion batteries: Li2VIII(PO4)(HPO4)

E. Boivin, C. Masquelier, L. Croguennec & J. N. Chotard

J. Inorg. Chem., in Press, May 2017


129. Understanding defects in battery materials through combined DFT/NMR studies: application to LiVPO4F

T. Bamine, F. Boucher, R. J. Messinger, E. Salager, M. Deschamps, C. Masquelier, L. Croguennec, M. Ménétrier, D. Carlier

J. Phys. Chem C, DOI: 10.1021/acs.jpcc.6b11747 (2017)


128. VIV disproportionation upon sodium extraction from Na3V2(PO4)2F3 observed by operando X-ray Absorption Spectroscopy and Solid State NMR

T. Broux, T. Bamine, L. Simonelli, L. Stievano, F. Fauth, M. Ménétrier, D. Carlier, C. Masquelier & L. Croguennec,

J. Phys. Chem C, DOI: 10.1021/acs.jpcc.6b11747 (2017)


127. Pathways to enhance lithium-ion conductivity in solid electrolytes: a mixed polyanion effect in the LISICON-type structure

Y. Deng, C. Eames, B. Fleutot, J.N. Chotard, E. Suard, C. Masquelier, S. Islam

ACS Applied Materials & Interfaces, DOI:10.1021/acsami.6b14402 (2017)


126. Oxidation under air of Tavorite LiVPO4F: influence of vanadyl-type defects on its electrochemical properties

E. Boivin, J. N. Chotard, M. Ménétrier, L. Bourgeois, T. Bamine, D. Carlier, F. Fauth, C. Masquelier, L. Croguennec

J. Phys. Chem. C, DOI: 10.1021/acs.jpcc.6b07342 (2016)


125. Strong impact of the oxygen content in Na3V2(PO4)2F3-yOy (0 <  y < 0.5) on their structural and electrochemical properties

T. Broux, T. Bamine, F. Fauth, L. Simonelli, M. Ménétrier, D. Carlier, C. Masquelier, L. Croguennec

Chem. Mater., DOI: 10.1021/acs.chemmater.6b02659 (2016)


124. Structural and Electrochemical Studies of a New Tavorite Composition: LiVPO4OH

E.  Boivin, J. N. Chotard, M. Ménétrier, L. Bourgeois, Tahya Bamine, D. Carlier, F. Fauth, E. Suard, C. Masquelier, L. Croguennec

J. Mater. Chem. A,  DOI: 10.1039/C6TA03339C (2016)


123. Spinel materials for Li-ion batteries, new insights from operando neutron and synchrotron X-Ray diffraction

M. Bianchini, F. Fauth, E. Suard, J. B.. Leriche, C. Masquelier, L. Croguennec 

Acta cryst., DOI: 10.1107/52052520615017199 (2015)


122. Discovery of a sodium-ordered form of Na3V2(PO4)3 below ambient temperature

J.N. Chotard, G. Rousse, R. David, O. Mentré, C. Masquelier,

Chem Mater., 27, 5982-5987 (2015) ; DOI: 10.1021/acs.chemmater.5b02092


121. Improving the energy density of Na3V2(PO4)3 – type positive electrodes through V / Al substitution

F. Lalère, V. Seznec, M. Courty, J. N. Chotard, C. Masquelier,

J. Mater. Chem. A, 3, 16198-16205 (2015), DOI : 10.1039/C5TA03528G


120. Structural and mechanistic insights into fast lithium-ion conduction in Li4SiO4-Li3PO4 solid electrolytes

Y. Deng, C. Eames, J. N. Chotard, F. Lalère, V. Seznec, S. Emge, O. Pecher, C. P. Grey, C. Masquelier, M. S. Islam

J. American Chem. Soc., (2015), DOI: 10.1021/jacs.5b04444 


119. Revealing Defects in Crystalline Lithium-Ion Battery Electrodes by Solid-State NMR: Applications to LiVPO4F

R. Messinger, M. Ménétrier, E. Salager, A. Boulineau, M. Duttine, D. Carlier, J. M. Ateba Mba, L. Croguennec, C. Masquelier, D. Massiot, M. Deschamps

Chem. Mater., 27, 5212-5221 (2015) ; DOI: 10.1021/acs.chemmater.5b01234


118. Singular structural and electrochemical properties in highly defective LiFePO4 powders

R. Amisse, M. Sougrati, L. Stievano, C. Davoisne, G. Dražič, R. Dominko, C. Masquelier

Chem. Mater., 27(12), 4261-4273 (2015) ; DOI: 10.1021/acs.chemmater.5b00470


117. Comprehensive investigation of the Na3V2(PO4)2F3 - NaV2(PO4)2F3 system by operando high resolution synchrotron X-ray diffraction

M. Bianchini, F. Fauth, E. Suard, C. Masquelier & L. Croguennec

Chem. Mater., 27(8), 3009-3020 (2015) ; DOI: 10.1021/acs.chemmater.5b00361


116. (NH4)0.75Fe(H2O)2[BP2O8]•0.25H2O, a Fe3+/Fe2+ mixed valence cathode material for Na battery exhibiting an helical structure

L. Tao, G. Rousse, M. T. Sougrati, J. N. Chotard, C. Masquelier

J. Phys. Chem. C, 119, 4540-4549 (2015) ; DOI: 10.1021/jp5117596 


115. Synthesis of Li2FeSiO4/Carbon Nano-Composites by Impregnation Method

S. Sun, C. M. Ghimbeu, Cathie Vix-Guterl, M.T. Sougrati, C. Masquelier, R. Janot

J. Power Sources, 284, 574-581 (2015) ; DOI: 10.1016/j.jpowsour.2015.03.028


114. Li-Rich Li1+xMn2-xO4 Spinel Electrode Materials: An Operando Neutron Diffraction study during Li+ extraction / insertion

M. Bianchini, L. Croguennec, E. Suard & C. Masquelier

J. Phys. Chem. C, 118(45), 25947-25955 (2014) ; DOI: 10.1021/jp509027g


113. One-pot synthesis of LiFePO4-carbon mesoporous composites for Li-ion batteries

S. Sun, C. Ghimbeu, R. Janot, J. M. LeMeins, A. Cassel, C. Davoisne, C. Masquelier, C. Vix-Guterl

Microporous and Mesoporous Materials, 198, 175-184 (2014) ; DOI : 10.1016/j.micromeso.2014.07.39


112. Na3V2(PO4)2F3 revisited: a high resolution diffraction study

M. Bianchini, N. Brisset, F. Fauth, F. Weill, E. Elkaim, E. Suard, C. Masquelier & L. Croguennec

Chem. Mater., 26(14), 4238-4247 (2014) ; DOI: 10.1021/cm501644g


111. Multiple phases in the ε-VPO4O - LiVPO4O - Li2VPO4O system: a combined solid state electrochemistry and diffraction structural study

M. Bianchini, J.M. Atebamba, P. Dagault, E. Bogdan, D . Carlier, E. Suard, C. Masquelier & L. Croguennec

J. Mater. Chem. A, 2, 10182-10192 (2014) ; DOI: 10.1039/C4TA01518E (2014)


110. Polymorphism in Li2MSiO4 (M = Fe, Mn): a variable temperature diffraction study

A. R. Armstrong, C. Sirisopanaporn, P. Adamson, J. Billaud, R. Dominko, C. Masquelier& P.G. Bruce

Z. Anorg. Allg. Chem., 640(6), 1043-1049 (2014) ; DOI: 10 1002/zaac.201400081(2014)


109. On the nature of phase transitions in tetragonal tungsten bronzes GdK2Nb5O15 ceramics

Y. Amira, Y. Gagou,D. Mezzane, M. Elaatmani, M. Courty, C. Masquelier, Y. Yu. Yuzyuk & M. El Marssi

J. Appl. Phys., 115, 064104 (2014)


108. Complex cation distribution in LiFeBO3

L. Tao, G. Rousse, D. Hanžel, G. Mali, R. Dominko, S. Levasseur & C. Masquelier

J. Mater. Chem A., 2(7), 2060-2070 (2014)


107. An All Solid State NASICON sodium Battery operating at 200°C

F. Lalère, J.B. Leriche, M. Courty, S. Boulineau, V. Viallet, C. Masquelier & V. Seznec

J. Power Sources, 247(1), 975-980 (2014)


106. Helicoïdal magnetic structure in LiFeAs2O7 : a neutron diffraction study

G. Rousse, C. Wurm, J. Rodriguez-Carvajal, C. Masquelier

Phys. Rev. B, 88, 214433 (2013)


105. A New Null Matrix Electrochemical Cell for Rietveld Refinements of in situ or operando neutron powder diffraction data,

M. Bianchini, J. B. Leriche, J.-L. Laborier, L. Gendrin, E. Suard, L. Croguennec & C. Masquelier,

J. Electrochem. Soc., 160(11), A2176-A2183 (2013)


104. Magnetic Structures of the Li-ion Battery Materials LiMBO3 (M = Fe, Co, Mn)

L. Tao, J. R. Neilson, B. C. Melot, T. M. McQueen, C. Masquelier, G. Rousse

Inorg. Chem., 52(20), 11966—11974 (2013)


103. Nonstochiometry in LiFe0.5Mn0.5PO4: structural and electrochemical properties

R. Amisse, S. Hamelet, D. Hanžel, R. Dominko, C. Masquelier

J. Electrochem. Soc., 160(9), A1446-A1450 (2013)


102. Towards high energy density sodium ion batteries through electrolyte optimization

A. Ponrouch, R. Dedryvère, D. Monti, A. E. Demet, J. M. Ateba Mba, L. Croguennec, C. Masquelier, P. Johansson, M. R. Palacín

Energy Environ. Sci., 6, 2361-2369 (2013)


101. Polyanionic (phosphates, silicates, sulphates,..) frameworks as electrode materials for rechargeable Li (or Na) batteries

C. Masquelier, L. Croguennec

Chem. Rev., 113(8), 6552 (2013)


100. Heterogeneous electrochemical behaviour of the lithium battery electrode LiFePO4

M. Zerrouki, G. Ouvrard, P. Soudan, B. Lestriez, C. Masquelier, M. Morcrette, S. Hamelet, J. Lesage, S. Belin, A.M. Flanck, F. Baudelet

J. Power Sources, 229, 16-21 (2013)


99. Synchrotron X-rays and neutrons as essential tools in Li battery research: examples of oxide, phosphate and silicate-based positive electrodes

C. Masquelier

European Physics Journal, 213, 213-224 (2012)


98. In-situ X-ray diffraction study of electrochemical insertion in Mg0.5Ti2(PO4)3 : an electrode material for lithium or sodium batteries.
P. Lavela, C. Vidal-Abarca, J.M. Ateba Mba, C. Masquelier, J. Tirado

J. Electrochem. Soc., 159(10), A1716-A1722 (2012)


97. Hydrothermal synthesis, silver decoration and electrochemistry of LiMPO4 (M=Fe, Mn, and Co) single-crystals

N. Recham, J. Oró-Solé, K. Djellab, M. R. Palacín, C. Masquelier, J-M. Tarascon

Solid State Ionics, 220, 47-52 (2012)


96. Lithium insertion or extraction from/into Tavorite-type LiVPO4F: an in situ X-Ray Diffraction Study

J. M. Ateba Mba, L. Croguennec, J. Barker, N.I.Basir, C. Masquelier

J. Electrochem. Soc., 159(8), A1171-A1175 (2012)


95. Synthesis and crystallographic study of homeotypic LiVPO4O and LiVPO4F

J. M. Ateba Mba, E. Suard, C. Masquelier, L. Croguennec

Chem. Mater. 24(6), 1223-1234 (2012)


94. X-ray diffraction, dielectric, conduction and Raman studies in Na0.925Bi0.075Nb0.925Mn0.075 ceramic

C. Chaker, Y. Gagou, N. Abdelmoula, J.-L. Dellis, C. Masquelier, M. El Marssi

J. Appl. Phys. 111, 04410 (2012)


93. Solid Electrolytes : Lithium ions on the fast track

C. Masquelier

Nature Materials , 10(9), 648-650 (2011)


92. Polymorphism in Li2(Fe,Mn)SiO4 : a combined diffraction and NMR study

C. Sirisopanaporn, R. Dominko, C. Masquelier, A. R. Armstrong, G. Mali, P. G. Bruce

J. Mater. Chem., DOI:10.1039/C1JM12845K (2011)


91. “Give Energy to Your Study”: Students Worldwide Gather in Europe To Design Future Materials for Energy Storage and Conversion

P. Simon, P. Knauth, J. L. Tirado, W. Wieczorek, J. Plocharski, A. Barnabé, J. M. Tarascon, C. Masquelier

J. Chem. Educ. 88, 1203-1026 ( 2011)


90. α- Na3M2(PO4)3 (M = Ti, Fe): Absolute cationic ordering in NASICON-type phases

H. Kabbour, D. Coillot, M. Colmont, C. Masquelier, O. Mentré

J. Am. Chem. Soc., 133(31), 11900-11903 (2011)


89. Electrochemical kinetic study of LiFePO4 using Cavity Microelectrode

J. Come, P.-L. Taberna, S. Hamelet, C. Masquelier,P. Simon

J. Electrochem. Soc., 158(10), 1-4 (2011)


88. Li2FeSiO4 polymorphs probed by 6Li MAS NMR and 57Fe Mössbauer spectroscopy

G.. Mali, C. Sirisopanaporn, C. Masquelier, D. Hanzel & R. Dominko

Chem. Mater., 23(11), 2735-2744 (2011)


87. Reversed Phase Composite Polymeric Electrolytes Based on Poly(oxyethylene)

J. S. Syzdek, M. Armand, P. Falkowski, M. Gizowska,M. Karzowicz, Y. Yukaszuk, M. Marcinek, A. Zalewska, M. Szafran, C. Masquelier, J. M. Tarascon, W. Wieczorek, Z. G. Zukowska

Chem. Mater., 23(7), 1785-1797 (2011)


86. Silicate cathodes for lithium batteries: alternatives to phosphates?

S. Islam, R. Dominko, C. Masquelier, C. Sirisopanaporn, R. A. Armstrong, P. G. Bruce

J. Mater. Chem., 21, 9811-9818 (2011)


85. Dependence of Li2FeSiO4 electrochemistry on structure

C. Sirisopanaporn, C. Masquelier, R.A. Armstrong, P.G. Bruce & R. Dominko

J. Am. Chem. Soc.,133, 12631265 (2011)


84. Existence of superstructures due to large amounts of Fe vacancies in LiFePO4-type framework

S. Hamelet, M. Casas-Cabanas, L. Dupont, C. Davoisne, J.M. Tarascon & C. Masquelier

Chem. Mater., 23(1), 32-38 (2011)


83. Linking Local Environments and Hyperfine Shifts: a Combined Experimental and Theoretical 31P and 7Li Solid–State NMR Study of Paramagnetic Fe(III) Phosphates and Pyrophosphates

J. Kim, D. S. Middlemiss, B. Y. X. Zhu, N. Chernova, C. Masquelier & C. P. Grey

J. Am. Chem. Soc., 132(47), 16825-16840 (2010)


82. On the origin of the electrochemical capacity in Li2Fe0.8Mn0.2SiO4

R. Dominko, C. Sirisopanaporn, C. Masquelier, D. Hanzel, I. Arcon & M. Gaberscek

J. Electrochem Soc, 157(12), A1309-A1316 (2010)


81. Crystal structure of a new polymorph of Li2FeSiO4

C. Sirisopanaporn, A. Boulineau, R. Dominko, R.D. Armstrong, P.G. Bruce & C. Masquelier

Inorg. Chem., 49(10), 7446-7451 (2010)


80. Polymorphism and structural defects in Li2FeSiO4

A. Boulineau, C. Sirisopanaporn, R. Dominko, A. R. Armstrong, P. G. Bruce& C. Masquelier

Dalton Transactions, 39(27), 6310-6316 (2010)


79. High temperature electrochemical performance of nanosized LiFePO4

F. Mestre-Aizpurua, S. Hamelet, C. Masquelier & R. Palacin

J. Power Sources, 195(19), 6897-6901 (2010)


78. An electrochemical cell for operando study of lithium batteries using synchrotron radiation

J.B. Leriche, S. Hamelet, J. Shu, M. Morcrette, C. Masquelier, G. Ouvrard, M. Zerrouki, P. Soudan, S. Belin, E. Elkaim, F. Baudelet

J. Electrochem. Soc., 157(5), A606-A610 (2010)


77. Crystal structures and sodium/silver distributions within the ionic conductors Na5Ag2Fe3(As2O7)4 and Na2Ag5Fe3(P2O7)4

Eric Quarez, Olivier Mentré, K. Djellab & C. Masquelier

New J. Chem., 34, 287-293 (2010)


76. Lithium insertion mechanism in crystalline and amorphous FePO4.nH2O

C. Delacourt, P. Poizot, D. Bonnin & C. Masquelier

J. Electrochem. Soc., 156(7), A595-A605 (2009)


75. The effects of moderate thermal treatments under air on LiFePO4-based nanopowders

S. Hamelet, P. Gibot, M. Casas Cabanas, D. Bonnin, C. Grey, J. Cabana, J. B. Leriche, J. Rodriguez Carvajal, M. Courty, S. Levasseur, P. Carlach, M. Van Thournout, J. M. Tarascon & C. Masquelier

J. Mater. Chem., 19, 3979-3991 (2009)


74. Comparative studies on the phase stability, electronic structure and topology of the charge density in the Li3XO4 (X = P, As, V) lithium orthosalt polymorphs

C. Frayret, C. Masquelier, A. Villesuzanne, M. Morcrette & J.M. Tarascon

Chem. Mater., 21(9), 1861-1874 (2009)


73. Crystal structures of new silver ion conductors Ag7Fe3(X2O7)4 (X = P, As)

E. Quarez, O. Mentré, Y. Oumellal & C. Masquelier

New J. Chem., 33, 998-1005 (2009)


72. Better electrode materials for Li-based batteries via diversified chemical approaches
N. Recham, M. Armand, R. Janot, C. Masquelier, L. Dupont, J.-M. Tarascon

Zeitschrift für anorganische und allgemeine Chemie, 634, 11 (2008)


71. Room-temperature single-phase Li insertion/extraction in nanoscale LixFePO4

P. Gibot, M. Casas-Cabanas, L. Laffont, S. Levasseur, P. Carlach, S. Hamelet, J-M. Tarascon & C. Masquelier,

Nature Materials, 7, 741-747 (2008)


69. Comparative study of the phase transition of Li1+xMn2−xO4 by anelastic spectroscopy and differential scanning calorimetry

A. Paolone, R. Cantellia, B. Scrosati, P. Reale, M. Ferretti and C. Masquelier

Electrochem. Comm. 8 (1), 113-117 (2006)


68. Study of the LiFePO4 / FePO4 two-phase system by high-resolution electron energy loss spectroscopy

L. Laffont, C. Delacourt, P. Gibot, M. Y. Wu, P. Kooyman, C. Masquelier & J.M. Tarascon
Chem. Mater., 18 (23): 5520-5529 (2006)


67. Size effects on carbon-free LiFePO4 powders: the key for superior energy density

C. Delacourt, P. Poizot & C. Masquelier

Electrochem. Solid State Lett. 9, A352 (2006)


64. Crystal chemistry of the olivine-type LixFePO4 system (0 < x < 1) between 25 and 370°C

Charles Delacourt, Juan Rodriguez-Carvajal, Bernd Schmitt, Jean-Marie Tarascon & Christian Masquelier

Solid State Sciences, 7, 1506-1516 (2005)


63. Synthesis, Phase Stability, and Electrochemically Driven Transformations in the LiCuO2-Li2CuO2 System

A. S. Prakash, D. Larcher, M. Morcrette, M. S. Hegde, J-B. Leriche, & C. Masquelier

Chem. Mater., 17(17), 4406-4415 (2005)


62. The existence of a temperature-driven solid solution for 0 < x < 1 in LixFePO4

C. Delacourt, P. Poizot, J.M. Tarascon & C. Masquelier

Nature Materials, 4, 254–260 (2005)


61. Towards the understanding of electrical limitations (electronic, ionic) in LiMPO4 (M = Fe, Mn) electrode materials

C. Delacourt, L. Laffont, R. Bouchet, C. Wurm, J.-B. Leriche, M Morcrette, J.-M. Tarascon & C. Masquelier

J . Electrochem. Soc., 152 (5) A913-A921 (2005)


60. Stabilization of an orthorhombic phase in LiMn2O4 by means of high pressure
A. Paolone, A. Sacchetti, P. Postorino, R. Cantelli, A. Congeduti, G. Rousse & C. Masquelier

Solid State Ionics, 176, 5-6, 635-639 (2005)


59. Various strategies to tune the ionic/electronic properties of electrode materials,

J. M. Tarascon, C. Delacourt, A. S. Prakash, M. Morcrette, M. S. Hegde, C. Wurm & C. Masquelier

J. Chem. Soc., Dalton Trans 2988-2994 (2004)


58. Low temperature preparation of optimized phosphates for Li-battery applications
C. Delacourt, C. Wurm, P. Reale, M. Morcrette & C. Masquelier

Solid State Ionics, 173, 1-4, 113-118 (2004)


57. Structural and Electrochemical Studies of orthorhombic Li2+xTiFe(PO4)3 and Li2+xTiCr(PO4)3

S. Patoux, G. Rousse, J.B. Leriche & C. Masquelier

Solid State Sciences, 6(10), 1113-1120 (2004)


56. MicroRaman spectroscopy on LiMn2O: warnings on laser-induced thermal decomposition
A. Paolone, A. Sacchetti, T. Corridoni, P. Postorino, R. Cantelli, G. Rousse & C. Masquelier

Solid State Ionics, 170, 1-2, 135-138 (2004)

55. Disproportionation of stoichiometric LiMn2O4 on annealing in oxygen

P. Strobel, G. Rousse, A. Ibarra Palos & C. Masquelier

J. Solid State Chem., 1-5, 177 (2004)


54. A one step low-temperature route for the preparation of electrochemically active LiMnPO4 powders

C. Delacourt, P. Poizot, M. Morcrette, J. M. Tarascon & C. Masquelier

Chem. Mater., 16(1), 93-99 (2004)


53. Synthesis and thermal behaviour of crystalline Hydrated Iron (III) Phosphates of interest as Positive Electrodes in Li Batteries

P. Reale, B. Scrosati, C. Delacourt, C. Wurm, M. Morcrette and C. Masquelier

Chem. Mater., 15(26), 5051-5058 (2003)


52. Magnetic structures of the triphylite LiFePO4 and of its delithiated form FePO4

G. Rousse, J. Rodriguez-Carvajal, S. Gwizdala, S. Patoux and C. Masquelier

Chem. Mater, 15(21), 4082-4090 (2003)


51. Structural and electrochemical studies of rhombohedral Na2TiM(PO4)3 and Li1.6Na0.4TiM(PO4)3 (M = Fe, Cr) phosphates

S. Patoux, G. Rousse, J.B. Leriche and C. Masquelier

Chem. Mater, 15(10), 2084-2093 (2003)


50. Evidence of a splitting of the Mn-O distance and of large lattice disorder in the charge ordered phase of LiMn2O4 obtained by EXAFS

A. Paolone, C. Castellano, R. Cantelli, G. Rousse and C. Masquelier

Phys. Rev. B, 68, 014108 (2003)


49. Development of potentiometric ion sensors based on insertion materials as sensitive elements

N. Le Poul, E. Baudrin, M. Morcrette, S. Gwizdala, C. Masquelier and J.M. Tarascon

Solid State Ionics, 8877 (2003) 1-10


48. In situ X-ray diffraction during lithium extraction from rhombohedral and monoclinic Li3V2(PO4)3

M. Morcrette, J.B. Leriche, S. Patoux, C. Wurm and C. Masquelier,

Elec. And Solid State Letters, 6(5) A80-A84 (2003)


47. A comparative structural and electrochemical study of monoclinic Li3Fe2(PO4)3 and Li3V2(PO4)3

S. Patoux, C. Wurm, G. Rousse, M. Morcrette and C. Masquelier,

J. Power Sources, 119-121, 278-284 (2003)


46. Effect of particle size on lithium intercalation into a-Fe2O3

D. Larcher, C. Masquelier, D. Bonnin, Y. Chabre, V. Masson, J. B. Leriche and J.M. Tarascon,

J . Electrochem. Soc., 150(1) A133-139 (2003)


44 Lithium insertion into titanium oxides, phosphates, silicates and sulfates

S. Patoux and C. Masquelier,

Chem. Mater.,14(12), 5057-5058 (2002)


43. In situ X-ray diffraction techniques as a powerful tool to improve battery electrode materials

M. Morcrette, Y. Chabre, G. Vaughan, G. Amatucci, J.B. Leriche, S. Patoux, C. Masquelier and J.M. Tarascon,

Electrochimica Acta, 47, 3137-3149 (2002)


42. Lithium insertion/extraction into/from LiMX2O7 compositions (M = Fe, V) prepared via a solution method

C. Wurm, M. Morcrette, G. Rousse, L. Dupont and C. Masquelier,

Chem. Mater.14(7), 2701-2710 (2002)


41. FePO4 . nH2Oand Fe4(P2O7)3 . nH2O : hydrated iron phosphates as 3 V positive electrodes in rechargeable lithium batteries

C. Masquelier, P. Reale, C. Wurm, M. Morcrette, L. Dupont and D. Larcher,

J . Electrochem. Soc. 149(8), A1037-A1044 (2002)


40. Chemical and electrochemical insertion of lithium in two allotropic varieties of NbPO5

S. Patoux and C. Masquelier,

Chem. Mater.14(5), 2334-2341 (2002)


39. A neutron diffraction study of the antiferromagnetic diphosphate LiFeP2O7

G. Rousse, C. Wurm, C. Masquelier andJ. Rodríguez-Carvajal,

Solid State Sciences, 4, 973-978 (2002)


38. A reversible lithium intercalation process in an ReO3-type structure : PNb9O25

S. Patoux, M. Dollé, G. Rousse and C. Masquelier,

J. Electrochem. Soc. 149(4), A391-A400 (2002)


37. On the way to the optimization of Li3Fe2(PO4)3 positive electrode materials

M. Morcrette, C. Wurm and C. Masquelier,

Solid State Sciences, 4, 239-246 (2002)


36. Magnetic structural studies of the two polymorphs of Li3Fe2(PO4)3 : analysis of the magnetic ground state from super-superexchange interactions

G. Rousse, J. Rodríguez-Carvajal, C. Wurm and C. Masquelier,

Chem. Mater., 13, 4527-4536 (2001)


35. Investigation of Positive Electrode Materials for Lithium Batteries by Means of X-ray and Neutron Diffraction

C. Masquelier, M. Morcrette and G. Rousse,

ESRF NewsLetter, pp 22-24, June 2001


34. On the role of defects in decreasing the extra 3.3/3.95 and 4.5 V redox steps in Li-Mn-O spinels

M. R. Palacin, G. Rousse, M. Morcrette, L. Dupont, C. Masquelier, Y. Chabre, M. Hervieu and J. M. Tarascon,

J. Power Sources, 4180, 1-4 (2001)


33. Crystal Structure of a new vanadium(IV) diphosphate : VP2O7, prepared by lithium extraction from LiVP2O7

G. Rousse, C. Wurm, M. Morcrette, J. Rodriguez-Carvajal, J. Gaubicher and C. Masquelier,

Int. J. Inorg. Mater., 3, 881-887 (2001)


32. A powder neutron diffraction investigation of the two rhombohedral NASICON analogs : g-Na3Fe2(PO4)3 and Li3Fe2(PO4)3

C. Masquelier, Calin Wurm, J. Rodríguez-Carvajal, J. Gaubicher, and L. Nazar,

Chem. Mater., 12(2), 525-532 (2000)


31. On the Origin of the 3.3V and 4.5V steps observed in LiMn2O4 spinels

M. R. Palacin, Y. Chabre, L. Dupont, M. Hervieu, P. Strobel, G. Rousse, C. Masquelier, M. Anne, G. Amatucci and J. M. Tarascon,

J. Electrochem. Soc. 147 (3) 845-853 (2000).


30. TEM studies: the key for understanding the origin of the 3.3V and 4.5V steps in LiMn2O4 based spinels

L. Dupont, M. Hervieu, G. Rousse, C. Masquelier, M.R. Palacín, Y. Chabre and J.M. Tarascon,

J. Solid State Chem. 155, 394-408 (2000).


29. Rhombohedral form of Li3V2(PO4)3 as a cathode in Li-ion batteries

J. Gaubicher, C. Wurm, G. Goward, C. Masquelier and L. Nazar,

Chem. Mater. 12, 3240-3242 (2000).


27. Cubic to orthorhombic transition in the stoichiometric spinel LiMn2O4.

G. Rousse, C. Masquelier, J. Rodriguez-Carvajal and M. Hervieu,

Elec. & Solid State Letters, 2 (1), 6-8 (1999).


26. Preparation of LiCoO2 and LiCo1-xFexO2 using hydrothermal reactions.

M. Tabuchi, K. Ado, H. Kobayashi, H. Sakaebe, H. Kageyama, C. Masquelier, M. Yonemura, A. Hirano and R. Kanno,

Journal of Materials Chemistry, 9, 199-204, (1999).


25. Infrared spectroscopy investigation of the charge ordering transition in LiMn2O4

A. Paolone, P. Roy, G. Rousse, C. Masquelier, J. Rodriguez-Carvajal,

Solid State Comm., 111, 453-458 (1999)


24. The relationships between phases and structures of lithium manganese spinels

R. Kanno, A. Kondo, M. Yonemura, R. Gover, Y. Kawamoto, M. Tabuchi, T. Kamiyama, C. Masquelier, G. Rousse,

Journal of Power Sources, 81-82, 542-546 (1999).


23. X-Ray study of the spinel LiMn2O4 at low temperatures

G. Rousse, C. Masquelier, J. Rodriguez-Carvajal, E. Elkaim, and J. P. Lauriat, J. L. Martinez

Chem. Mater., 11(12), 3629-3635 (1999)


22. New cathode materials for rechargeable lithium batteries : the 3-D framework structures Li3Fe2(XO4)3.

C. Masquelier, A. K. Padhi, K. S. Nanjundaswamy and J. B. Goodenough,

J. Solid State Chem., 135, 228-234 (1998).


21. Synthesis of LiMnO2 with NaMnO2 type structure by a mixed-alkaline hydrothermal reaction.

M. Tabuchi, K. Ado, H. Kobayashi, H. Kageyama, C. Masquelier, A. Kondo and R. Kanno,

J. Electrochem. Soc. 145 [4], L49-L52 (1998).


20. Effect of cation arrangement on the magnetic properties of lithium ferrites (LiFeO2) prepared by hydrothermal reaction and post-annealing method.

M. Tabuchi, S. Tsutsui, C. Masquelier, R. Kanno, K. Ado, I. Matsubara, S. Nasu and H. Kageyama,

J. Solid State Chem. 140, 159-167 (1998).


19. Magnetic properties of metastable lithium iron oxides obtained by solvothermal / hydrothermal reaction

M. Tabuchi, H. Kobayashi, I. Matsubara, H. Kageyama, S. Tsutsui, S. Nasu, C. Masquelier, A. Hirano and R. Kanno,

J. Solid State Chem. 141, 554-561 (1998).


18. Electronic crystallization in a lithium battery material: columnar ordering of electrons and holes in the spinel LiMn2O4

J. Rodriguez-Carvajal, G. Rousse, C. Masquelier and M. Hervieu,

Phys. Rev. Letters, 81, 1460, Nov. 23 (1998)


17. Effect of structure on the Fe3+/Fe2+ redox couple in iron phosphates

A.K. Padhi, K. S. Nanjundaswamy, C. Masquelier, S. Okada, and J. B. Goodenough,

J. Electrochem. Soc. 144(5), 1609-1614 (1997)


16. Mapping of transition-metal redox energies in phosphates with NASICON structure by lithium intercalation

A.K. Padhi, K. S. Nanjundaswamy, C. Masquelier, J. B. Goodenough,

J. Electrochem. Soc. 144(8), 2581-2588 (1997)


15. Characterization of Li1-dMn2-2dO4 defect spinel materials by their phase transition, magnetic and electrochemical properties

M. Tabuchi, C. Masquelier, H. Kobayashi, R. Kanno, Y. Kobayashi, Y. Maki, H. Kageyama and O. Nakamura,

J. Power Sources, 68, 623-628 (1997)


14. Electrochemical and magnetic properties of lithium manganese oxide spinels prepared by oxidation at low temperature of hydrothermally obtained LiMnO2

M. Tabuchi, K. Ado, C. Masquelier, I. Matsubara, H. Kageyama, R. Kanno, H. Kobayashi, and O. Nakamura,

Solid State Ionics, 89, 53-63 (1996)


13. Chemical and magnetic characterization of spinel materials in the LiMn2O4 - Li2Mn4O9 - Li4Mn5O12 system

C. Masquelier, M. Tabuchi, K. Ado, R. Kanno, Y. Kobayashi, Y. Maki, O. Nakamura, and J. B. Goodenough,

J. Solid State Chem. 123, 255-266 (1996)


12. Li+/Na+ exchange from NaFeO2 using hydrothermal reaction

M. Tabuchi, C. Masquelier, T. Takeuchi, I. Matsubara, T. Shirane, R. Kanno, H. Sakaebe, and O. Nakamura,

Solid State Ionics, 90, 129-132 (1996)


11. Characteristics of 3D framework cathodes with (XO4)n- polyanions

S. Okada, Y. Sakurai, J. Yamaki, K. S. Nanjundaswamy, A. K. Padhi, C. Masquelier and J. B. Goodenough,

Prog. in Lithium Ion Batteries, Edit. M. Yoshio, M. Thackeray and A. Kozawa, (1996)


10. Crystal structure of Na7Fe4(AsO4)6 and Na3Al2(AsO4)3 ; two sodium ion conductors structurally related to II-Na3Fe2(AsO4)3

C. Masquelier, F. d'Yvoire and G. Collin,

J. Solid State Chem. 118, 33-42 (1995)


9. Effect of content of BaTiO3 surface cubic layer on the ionic conductivity enhance-ment in composite solid electrolytes

T. Takeuchi, K. Ado, Y. Saito, M. Tabuchi, C. Masquelier and O. Nakamura,

Solid State Ionics, 79, 325-330 (1995)


8. Preparation of AFeO2 (A = Li, Na) by hydrothermal method

M. Tabuchi, K. Ado, H. Sakaebe, C. Masquelier, H. Kageyama and O. Nakamura,

Solid State Ionics, 79, 220-226 (1995)


7. Chemistry and structure analysis in the Li4+xBxSi1-xO4 solid solution

C. Masquelier, H. Kageyama, T. Takeuchi, Y. Saito and O. Nakamura,

J. Power Sources, 54, 448-451 (1995)


6. Influence of the preparation process on the cation transport properties of Li4+xMxSi1-xO4 (M = B, Al) solid electrolytes

C. Masquelier, M. Tabuchi, T. Takeuchi, W. Soizumi, H. Kageyama and O. Nakamura,

Solid State Ionics, 79, 98-105 (1995)


5. A new family of sodium ion conductors, the diphosphates and diarsenates Na7M3(X2O7)4 (M=Al, Ga ,Cr ,Fe, X=P, As)

C. Masquelier, F. d'Yvoire, E. Bretey, P. Berthet and C. Peytour,

Solid State Ionics, 67, 183-189 (1994)


4. Analysis of double layered structure of submicron BaTiO3 grains using equivalent circuit model

T. Takeuchi, K. Ado, T. Asai, H. Kageyama, K. Honjo, Y. Saito, C. Masquelier and O. Nakamura,

J. Ceram. Soc. Japan, International Edition, 102, No. 12, 1178-1181 (1994)


3. Thickness of the cubic surface phase on baryum titanate fine particles

T. Takeuchi, K. Ado, T. Asai, H. Kageyama, Y. Saito, C. Masquelier and O. Nakamura,

J. American Ceramic Society, 77, 1665-1668 (1994)


2. Crystal structure of the sodium ion conductor α-Na7Fe3(P2O7)4 : evidence of a long-range ordering of the Na+Ions

C. Masquelier, F. d'Yvoire and N. Rodier,

J. Solid State Chem. 95, 156-167 (1991)


1. Structure of the sodium ion conductor Na7Fe3(As2O7)4

C. Masquelier, F. d'Yvoire and N. Rodier,

Acta Cryst. C 46, 1584-1587 (1990)


May 30th, 2017: Attending the 8th ICE Conference in Nagoya, JAPAN 


February 15th, 2017: New Application of MESC Consortium for ERASMUS + EMJMD.


February 5th, 2017: the LRCS moves to its new building, the HUB of the RS2E French Network on Electrochemical Energy Storage.


February 5th, 2017: Paper #2 of Thibault BROUX, on VIV disproportionation in NVPF upon charge, accepted in ACS J. Phys. Chem. C


February 1st, 2017: Paper #2 of Yue DENG, on mixed anion effect in solid electrolytes, accepted in ACS Applied Materials & Interfaces


October 24th, 2016 : Paper #2 of Edouard BOIVIN, on LiVPO4(F,O) accepted in J. Phys. Chem. C.


October 6th, 2016 : Paper #1 of Thibault BROUX on Na3V2(PO4)2F3 accepted in Chem. Mater.


October 5th, 2016 : The Nobel Prize for Chesmistry is attributed to Jean-Pierre SAUVAGE from Strasbourg.


June 28-29, 2016 : ERAMUS + Meeting in Brussels on "Mastering Joint Excellence under ERASMUS MUNDUS" 


June 14-18, 2016 : IMLB 2016 in Chicago, 1800 attendees......


April 12-15, 2016 : Proposals Subcommittees and Scientific Council at ILL, Grenoble, FRANCE


March. 22, 2016 : Talk at IBA Conference, Nantes, France


Feb. 18, 2016 : Application of M.E.S.C. for ERASMUS + re-accreditation ......


Dec. 5, 2015 : Interview of Mathieu MORCRETTE, Director of LRCS, in "Agir en Picardie".



Nov. 23-25, 2015 :CNRS-sponsored ANF Chimie du Solide, organized in Caen, France.


Nov. 9, 2015 : PhD Defense of Fabien LALERE in UPJV Amiens 


Oct. 23, 2015 : PhD Defense of Matteo BIANCHINI in UPJV Amiens 


Sept. 15, 2015 : Graduation Ceremony in Amiens of Class#10 of M.E.S.C. Master Course.


Sept. 2, 2015 : invited Talk at European Conference on Neutron Scattering, Zaragoza, Spain


August 7, 2015 : New Crystal Structure of Na3V2(PO4)3 published in Chem. Mater.


July 1, 2015 : Yue DENG's first paper on Li4SiO4-Li3PO4 is published in JACS.


July 1, 2015 : Invited talk at ICMAT Singapore on highly defective LiFePO4 powders.


June 16, 2015 : Fabien LALERE gives a talk in SSI Conference, Keyston, USA


June 4, 2015 : Matteo BIANCHINI is the ECS Battery Student Award winner for 2015


June 1, 2015 : Robin AMISSE's paper on highly defective LiFePO4 accepted in Chemistry of Materials 


Nov 24, 2014 : the www site is launched. There is in particular a very convenient Job section.


July 23, 2014 : Visit the www site of Nature related to CRYSTALLOGRAPHY, MILESTONES


July 11, 2014 : HDR Defense of Joël GAUBICHER, IMN Nantes, France


June 15-18 : EPDIC Conference in Aarhus, Denmark.


June 7-12, 2014 : IMLB conference, Como, Italy


May 6, 2014 : Comité de Sélection, Poste 33MCF0269, Amiens


April 16th, 2014 : Conseil Académique à l'UPJV Amiens.


April 2-4, 2014 : Power our Future at CIC Energigune, SPAIN


March 18 & 19, 2014 : ILL Subcommittees for experiments, Grenoble, FRANCE 


March 3-7, 2014 : IBA Meeting in Brisbane, Australia


Feb. 24-25, 2014 : Meeting of the French RS2E in Lyon, FRANCE.


Feb. 11-13, 2014 : Meeting of the MESC Consortium in Marseille for the Selection of CLass#11 (2014-2016)


February 7, 2014 : All Solid State Battery Meeting of the RS2E.


February 7, 2014 : Na-ion Group Meeting of the RS2E


January 24, 2014 : Li-Ion Group Meeting of the RS2E in Collège de France, Paris


January  23, 2014 : Prof. J.M. TARASCON gives his Inaugural Lecture at College de France, Paris

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